Diffraction Structure — Bimetal MOF nanosheets as efficient anode materials for lithium-ion batteries

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Post-cycling FTIR, PXRD, SEM, and TEM

Infrared spectroscopy X-ray diffraction and scattering Scanning electron microscopy Transmission electron microscopy

Co1/2Fe1/2-MOF LIB anode electrode · Electrode

Co1/2Fe1/2-MOF electrode inspected in discharged, charged, pristine, and cycled states.

Geometry: cycled MOF/carbon/binder electrode
Context: cycled electrode
Measurement source: p010-p011 / article pp.10106-10107 · Results and discussion · Fig. 9

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co1/2Fe1/2-MOF becomes amorphous after cycling	No visible diffraction peaks after cycling; lost long-range organization and became amorphous	—	—	Text Qualitative	p010-p011 / article pp.10106-10107 · Results and discussion · Fig. 9b
Co1/2Fe1/2-MOF morphology after cyclingMarked as a best value within this paper	No pulverization or fractures after cycles	—	—	Text Qualitative	p011 / article p.10107 · Results and discussion · Fig. 9c-d

Supplemental XRD, SEM, and TEM-SAED on dried/cycled Co1/2Fe1/2-MOF electrode materials

X-ray diffraction and scattering Scanning electron microscopy Transmission electron microscopy

Co1/2Fe1/2-MOF LIB anode electrode · Electrode

Rendered SI shows XRD of dried Co1/2Fe1/2-MOF electrode material, SEM of dried electrode material, TEM-SAED of Co1/2Fe1/2-MOF, and XRD/SEM after 10 cycles.

Geometry: electrode material
Context: dried and cycled Co1/2Fe1/2-MOF electrode
Measurement source: p001-p003 · Supplementary Information · Fig. S1-S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co1/2Fe1/2-MOF XRD after 10 cycles	XRD of Co1/2Fe1/2-MOF after 10 cycles shown in Fig. S5; broad/amorphous pattern in rendered SI	—	—	Visual Estimate Qualitative	p003 · Supplementary Information · Fig. S5
TEM-SAED purity indication for Co1/2Fe1/2-MOF	TEM-SAED showed no obvious lattice fringes belonging to iron-rich or cobalt-rich secondary phases	—	—	Text Qualitative	p004 / article p.10100 · Results and discussion · Fig. S3

Powder X-ray diffraction (PXRD/XRD), Bruker D8 Advance, Cu-Ka radiation

X-ray diffraction and scattering

CoxFe1-x-MOF powder/nanosheet series · Nanosheet

Patterns collected for CoxFe1-x-MOF powders; Fig. S1 reportedly includes dried Co1/2Fe1/2-MOF electrode material.

Context: pristine powder series
Measurement source: p003 / article p.10099 · Results and discussion · Fig. 1a; Fig. S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
XRD structural framework retained across CoxFe1-x-MOF series	CoxFe1-x-MOFs retain a consistent structural framework	—	—	Text Qualitative	p003 / article p.10099 · Results and discussion · Fig. 1a