Microscopy Morphology — Morphologies of thienyl based bimetallic metal-organic frameworks controlled by solvents for high specific capacitance supercapacitor

Measurement evidence

Microscopy Morphology

Morphologies of thienyl based bimetallic metal-organic frameworks controlled by solvents for high specific capacitance supercapacitor · Song S., Ma X., Zhang B. et al. · Journal of Energy Storage · 2022 · 103627

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SI XRD, FT-IR, SEM and TEM rendered-page review

PTA-NC MOF · Powder

PTA-NC MOF comparison sample characterised by XRD (Fig. S1), FT-IR (Fig. S2), SEM (Fig. S3) and TEM (Fig. S4).

Context
pristine comparison powder
Measurement source
1-3 · Supporting information · Figures S1-S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PTA-NC MOF SEM morphologyaggregated rough particles/spheroids; scale bars 10 um and 500 nmVisual Estimate
Qualitative
2 · Supporting information · Figure S3
PTA-NC MOF TEM morphologydark spherical/aggregated particles with a 500 nm high-magnification scale barVisual Estimate
Qualitative
3 · Supporting information · Figure S4
PTA-NC MOF dominant XRD low-angle peakdominant peak near 8-9 degrees 2theta in SI Fig. S1approximatelyFigure Axis
Approximate
1 · Supporting information · Figure S1

Field-emission SEM (FE-CHEM, Quaint 250FEG)

E-NCT MOF · Nanosheet

SEM images for D-NCT, M-NCT and E-NCT morphology and size.

Context
pristine powder solvent variants
Measurement source
4 · 3.1. Structural and morphology characterization · Figure 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
D-NCT spherical particle sizeseveral hundred nanometers to 1 um to 3 umText
Range
4 · 3.1. Structural and morphology characterization · Figure 2a,d,g
E-NCT sheet lateral size1 um to 5 umText
Range
4 · 3.1. Structural and morphology characterization · Figure 2c,f,i

TEM (JEOLJEM 2100, 100 kV)

E-NCT MOF · Nanosheet

TEM images for D-NCT, M-NCT and E-NCT microstructure.

Context
pristine powder solvent variants
Measurement source
5 · 3.1. Structural and morphology characterization · Figure 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TEM solvent morphology trendDMF: solid spherical; MeOH: amorphous between spherical and flake; EtOH: sheet-likeText
Qualitative
5 · 3.1. Structural and morphology characterization · Figure 3