Microscopy Morphology — Copper-Metal Organic Frameworks Electrodeposited on Carbon Paper as an Enhanced Cathode for the Hydrogen Evolution Reaction

Measurement evidence

Microscopy Morphology

Copper-Metal Organic Frameworks Electrodeposited on Carbon Paper as an Enhanced Cathode for the Hydrogen Evolution Reaction · Li X.-F., Lu M.-Y., Yu H.-Y. et al. · ChemElectroChem · 2019 · 4507-4510

5 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM

Cu nanoparticle/carbon paper intermediate · Electrode

SEM images of copper nanoparticles deposited on carbon paper.

Context
composite intermediate
Measurement source
SI p004 · Figure S1 discussion · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu nanoparticle sizeabout 200-300 nmrange 200-300 nm; midpoint stored as value_numericText
Range
SI p004 · Figure S1 discussion · Figure S1

SEM

HKUST-1 ED on carbon paper · Electrode

SEM of electrodeposited HKUST-1 on carbon paper.

Context
target composite electrode
Measurement source
4508 · Results · Figure 1a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
HKUST-1 ED particle sizeMarked as a best value within this paperabout 500 nmText
Approximate
4508 · Results · Figure 1a,b

SEM

HKUST-1 HT powder/crystals · Powder

SEM of hydrothermal HKUST-1 comparison particles.

Context
pristine framework control
Measurement source
4508 · Results · Figure 1c,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
HKUST-1 HT particle sizeabout 20 um20000 nmText
Approximate
4508 · Results · Figure 1c,d

SEM after HER

HKUST-1 ED on carbon paper · Electrode

SEM images of HKUST-1 ED after HER catalysis.

Context
target composite electrode after HER
Measurement source
SI p005 · Figure S5 · Figure S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Morphology after HERoctahedral structure still remains on carbon paperText
Qualitative
4509 · Results · Figure S5

TEM and elemental mapping / EDS

HKUST-1 ED on carbon paper · Electrode

TEM at 200 kV and elemental mapping of HKUST-1 ED.

Context
target composite electrode
Measurement source
4508 · Results · Figure 1e-i
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Elemental mapping uniformityCu, O and C elements distributed uniformlyText
Qualitative
4508 · Results · Figure 1f-i