Other — Synthesis of millimeter-scale ZIF-8 single crystals and their reversible crystal structure changes

Measurement evidence

Other

Synthesis of millimeter-scale ZIF-8 single crystals and their reversible crystal structure changes · Alowasheeir A., Torad N.L., Asahi T. et al. · Science and Technology of Advanced Materials · 2024 · 2292485

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis (TG), Rigaku TG8120

as-synthesised SC-ZIF-8 single crystals · Single Crystal

Heated from room temperature to 1000 degC under nitrogen at 10 degC min-1.

Atmosphere
nitrogen
Context
thermal stability of pristine SC-ZIF-8
Measurement source
PDF p004 / article p3 · 2.3 Characterization; Results and discussion · Figure 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Third TG decomposition region upper temperaturethird weight reduction continues until 860 degCText
Exact Reported
PDF p006 / article p5 · Results and discussion · Figure 4
Second TG weight loss attributed to DEF removal25.0% weight loss persisting until 445 degCText
Exact Reported
PDF p006 / article p5 · Results and discussion · Figure 4
Internal DEF persistence temperaturesolvents can persist until 445 degC (718 K)718 KText
Exact Reported
PDF p006 / article p5 · Results and discussion · Figure 4; Table 1
First TG weight loss attributed to surface water2.2% weight loss up to 220 degCText
Exact Reported
PDF p006 / article p5 · Results and discussion · Figure 4