Porosity — Synthesis of millimeter-scale ZIF-8 single crystals and their reversible crystal structure changes

Measurement evidence

Porosity

Synthesis of millimeter-scale ZIF-8 single crystals and their reversible crystal structure changes · Alowasheeir A., Torad N.L., Asahi T. et al. · Science and Technology of Advanced Materials · 2024 · 2292485

1 measurement group · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption-desorption isotherms; BET and NLDFT analysis

SC-ZIF-8 sample activated for N2 adsorption · Single Crystal

Measured at 77 K on Quantachrome Autosorb gas sorption system after 150 degC activation for 24 h.

Temperature
77
Atmosphere
N2
Context
activated pristine SC-ZIF-8 porosity
Measurement source
PDF p004 / article p3 · 2.3 Characterization; Results and discussion · Figure 2(b)
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Approximate N2 adsorbed volume near P/P0 = 1about 430 cm3 g-1 STP near P/P0 = 1visual estimate from plotted axisFigure Axis
Approximate
PDF p004 / article p3 · Results and discussion · Figure 2(b)
N2 isotherm typetypical type I isotherm characteristics of microporous materialsText
Qualitative
PDF p004 / article p3 · Results and discussion · Figure 2(b)
Pore volume0.62 cm3 g-1Text
Exact Reported
PDF p005 / article p4 · Results and discussion · Figure 2(b)
Maximum NLDFT pore width25 Angstrom upper bound of 10-25 Angstrom rangeText
Range
PDF p005 / article p4 · Results and discussion · Figure 2(b)
Minimum NLDFT pore width10 Angstrom lower bound of 10-25 Angstrom rangeText
Range
PDF p005 / article p4 · Results and discussion · Figure 2(b)
SI Table S1 BET entry for this workMarked as a best value within this paperDEF, 120 degC, 72 h; BET 1681 m2 g-1SI Table
Exact Reported
SI rendered p003 · Supplementary Tables · Table S1
BET surface areaMarked as a best value within this paper1681 m2 g-1Text
Exact Reported
PDF p005 / article p4 · Results and discussion · Figure 2(b); Table S1