Complete recipeSource: Main
Route 1: Solvothermal
PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8
Metal precursors350 mg Zn(NO3)2.6H2O
Linker precursors200 mg 2-methylimidazole
Solvents15 mL N,N-diethylformamide (DEF); DMF wash and storage solvent
Additives60 uL of 70% HNO3 solution
Atmospherenot specified
Temperature120
Time72
Work-upCrystals collected through filtration and washed with DMF; subsequently stored in DMF at room temperature.
ActivationNo synthesis activation reported; separate N2 sorption sample was treated at 150 degC for 24 h before measurement.
Scalability contextProduces millimetre-scale single crystals reaching about 1 mm; some cubic unevolved crystals remained after 72 h.
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Zn(NO3)2.6 H2O | 350 mg | PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8 |
| Linker | 2-methylimidazole | 200 mg | PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8 |
| Solvent | N,N-diethylformamide (DEF) | 15 mL | PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8 |
| Acid | HNO3 solution | 60 uL · 70% | PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8 |
| Solvent | N,N-dimethylformamide (DMF) | wash and storage solvent | PDF p003 / article p2 · 2.2 Synthesis of SC-ZIF-8 |