Diffraction Structure — Superexchange Charge Transport in Loaded Metal Organic Frameworks

Measurement evidence

Diffraction Structure

Superexchange Charge Transport in Loaded Metal Organic Frameworks · Neumann T., Liu J., Wachter T. et al. · ACS Nano · 2016 · 7085-7093

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Out-of-plane XRD

F4-TCNQ-loaded HKUST-1 SURMOF, 5 spray cycles · Thin Film

Representative 5 spray-cycle F4-TCNQ-loaded SURMOF compared with pristine film.

Context
loaded sample compared with pristine control
Measurement source
7089 · Results and Discussion · Figure 4b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Framework crystallinity after F4-TCNQ loadingno change in SURMOF orientation or crystallinityText
Qualitative
7089 · Results and Discussion · Figure 4b

Out-of-plane XRD

Pristine HKUST-1 SURMOF, 5 spray cycles · Thin Film

Bruker D8 Advance theta-theta geometry, Cu K alpha radiation, 5-25 degree 2theta, 0.024 degree step, 16.4 s per step.

Context
pristine HKUST-1 SURMOF structural control
Measurement source
S3 · 1.5 Basic characterization · Figure 4a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
HKUST-1 SURMOF (111) Bragg peak2theta = 5.83 degreesText
Exact Reported
7089 · Results and Discussion · Figure 4a,b
HKUST-1 SURMOF (222) Bragg peak2theta = 11.68 degreesText
Exact Reported
7089 · Results and Discussion · Figure 4a,b
HKUST-1 SURMOF (333) Bragg peak2theta = 17.58 degreesText
Exact Reported
7089 · Results and Discussion · Figure 4a,b
HKUST-1 SURMOF high-angle Bragg peak2theta = 23.56 degreesText
Exact Reported
7089 · Results and Discussion · Figure 4a,b

Out-of-plane XRD

TCNQ-loaded HKUST-1 SURMOF, 5 spray cycles · Thin Film

Representative 5 spray-cycle TCNQ-loaded SURMOF compared with pristine film.

Context
loaded sample compared with pristine control
Measurement source
7089 · Results and Discussion · Figure 4a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Framework crystallinity after TCNQ loadingno change in SURMOF orientation or crystallinityText
Qualitative
7089 · Results and Discussion · Figure 4a