Microscopy Morphology — Superexchange Charge Transport in Loaded Metal Organic Frameworks

Measurement evidence

Microscopy Morphology

Superexchange Charge Transport in Loaded Metal Organic Frameworks · Neumann T., Liu J., Wachter T. et al. · ACS Nano · 2016 · 7085-7093

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

AFM height profiling

Pristine HKUST-1 SURMOF, 5 spray cycles · Thin Film

Height profile across chemically etched SURMOF edge; tapping mode, Multimode Bruker J scanner, 0.4 Hz, ambient laboratory conditions.

Temperature
294-297
Atmosphere
ambient laboratory conditions
Context
pristine thickness series
Measurement source
S3-S5 · 1.5; 2.1.1 Thickness evaluation · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pristine HKUST-1 SURMOF thickness, 10 cycles69.4 +/- 8.5 nm+/- 8.5 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3
Pristine HKUST-1 SURMOF thickness, 5 cycles44.7 +/- 3.9 nm+/- 3.9 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3
Pristine HKUST-1 SURMOF thickness, 7 cycles57.1 +/- 5.6 nm+/- 5.6 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3

AFM height profiling

TCNQ-loaded HKUST-1 SURMOF, 5 spray cycles · Thin Film

Height profile across chemically etched SURMOF edge for TCNQ-loaded thickness series.

Temperature
294-297
Atmosphere
ambient laboratory conditions
Context
TCNQ-loaded thickness series
Measurement source
S5 · 2.1.1 Thickness evaluation · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
F4-TCNQ-loaded HKUST-1 SURMOF thickness evaluationno thickness evaluation performed; assigned by spray-cycle countText
Qualitative
S10 · 2.3.1 Thickness evaluation
TCNQ-loaded HKUST-1 SURMOF thickness, 10 cycles62.3 +/- 7.3 nm+/- 7.3 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3
TCNQ-loaded HKUST-1 SURMOF thickness, 5 cycles33.3 +/- 3.0 nm+/- 3.0 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3
TCNQ-loaded HKUST-1 SURMOF thickness, 7 cycles53.2 +/- 4.1 nm+/- 4.1 nmText
Exact Reported
S5 · 2.1.1 Thickness evaluation · Figure S3