N2 sorption at 77 K; BJH and Horvath-Kawazoe pore-size analysis
3 · Powder
Nitrogen sorption after dehydration under vacuum at 393 K for 12 h.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Sample 1 Cage B accessible pore volume after HPW loading | about 0.06 nm^3 | — | — | Text Approximate | main p.4 · Results and discussion · Fig. S5 |
| Sample 1 unchanged Cage A pore size | 1.96 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |
| Sample 1 HPW-loaded Cage B pore size | 0.48 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |
| Sample 2 HPW-loaded Cage A pore size | 0.45 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |
| Sample 2 Cage A accessible pore volume after HPW loading | about 0.05 nm^3 | — | — | Text Approximate | main p.4 · Results and discussion · Fig. S5 |
| Sample 3 broad pore-size peak | centred at 0.47 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |
| MIL-101 Cage A pore size | 1.98 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |
| MIL-101 Cage B pore size | 2.38 nm | — | — | Text Exact Reported | main p.4 · Results and discussion · Fig. S5 |