Diffraction Structure — Synthesis of a novel double-ligand nickel conductive metal–organic framework material and its electrochemical characterization for supercapacitors

Measurement evidence

Diffraction Structure

Synthesis of a novel double-ligand nickel conductive metal–organic framework material and its electrochemical characterization for supercapacitors · Wang H., Zhu C., Wu M. et al. · Journal of Materials Science · 2021 · 2517-2527

2 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction (XRD, 9 kW/SmartLab)

Ni-MOF green powder · Powder

Experimental PXRD compared with simulated XRD spectrum for Ni-MOF.

Context
pristine Ni-MOF framework
Measurement source
4-5 · Structure and morphology / Materials characterization · Figure 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD phase agreementExperimental diffraction peaks are basically the same as simulated XRD spectrum for Ni-MOF.Text
Qualitative
4 · Structure and morphology · Figure 2a

single-crystal X-ray diffraction

Ni-MOF green powder · Powder

Crystal structure solution of Product 1 / Ni-MOF.

Context
pristine Ni-MOF framework
Measurement source
4 · Structure and morphology · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-N bond length range2.133(15) to 2.391(17) Arange 2.133(15)-2.391(17)Text
Range
4 · Structure and morphology · Figure 1
Ni-Ni distance3.50 AText
Exact Reported
4 · Structure and morphology · Figure 1
Ni-O bond length range2.133(15) to 2.391(17) Arange 2.133(15)-2.391(17)Text
Range
4 · Structure and morphology · Figure 1
space groupchiral orthorhombic P21212Text
Exact Reported
4 · Structure and morphology · Figure 1
framework dimensionalityone-dimensional (1D) MOFText
Exact Reported
4 · Structure and morphology · Figure 1