Spectroscopy — Fabrication of high-performance supercapacitor of surface-engineered ZIF-8 for energy storage applications

Measurement evidence

Spectroscopy

Fabrication of high-performance supercapacitor of surface-engineered ZIF-8 for energy storage applications · Karim M.R., Choi C.-H., Mohammad A. et al. · Journal of Energy Storage · 2024 · 112199

4 measurement groups · 24 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XPS peak table and atomic composition

1-Ag@ZIF-8 · Powder

1-Ag@ZIF-8 XPS composition from SI Table S1; columns Peak BE, FWHM, Area(P) CPS.eV and Atomic %.

Context
Ag@ZIF-8 composite sample
Measurement source
4 · Table S1 · Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag3d atomic percentage1.78 %SI Table
Exact Reported
4 · Table S1 · Table S1
Ag3d peak binding energy367.27 eVSI Table
Exact Reported
4 · Table S1 · Table S1
C1s atomic percentage44.39 %SI Table
Exact Reported
4 · Table S1 · Table S1
N1s atomic percentage13.76 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p atomic percentage13.62 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p peak binding energy1021.35 eVSI Table
Exact Reported
4 · Table S1 · Table S1
XPS Ag concentration in 1-Ag@ZIF-81.78 %SI Table
Exact Reported
4 · Table S1 · Table S1

XPS peak table and atomic composition

2-Ag@ZIF-8 · Powder

2-Ag@ZIF-8 XPS composition from SI Table S1; columns Peak BE, FWHM, Area(P) CPS.eV and Atomic %.

Context
Ag@ZIF-8 composite sample
Measurement source
4 · Table S1 · Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag3d atomic percentage2.79 %SI Table
Exact Reported
4 · Table S1 · Table S1
Ag3d peak binding energy367.41 eVSI Table
Exact Reported
4 · Table S1 · Table S1
C1s atomic percentage50.12 %SI Table
Exact Reported
4 · Table S1 · Table S1
N1s atomic percentage12.6 %SI Table
Exact Reported
4 · Table S1 · Table S1
O1s atomic percentage26.49 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p atomic percentage7.99 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p peak binding energy1021.28 eVSI Table
Exact Reported
4 · Table S1 · Table S1
XPS Ag concentration in 2-Ag@ZIF-8Marked as a best value within this paper2.79 %SI Table
Exact Reported
4 · Table S1 · Table S1

XPS survey and high-resolution Zn 2p, Ag 3d and O 1s spectra

2-Ag@ZIF-8 · Powder

Binding energies normalised to C 1s at 284.8 eV; results discussed for ZIF-8, 1-Ag@ZIF-8 and 2-Ag@ZIF-8.

Context
Ag-decorated ZIF-8 compared with pristine ZIF-8; sample key assigned to highest-loading target because Ag-specific results focus on Ag@ZIF-8.
Measurement source
3-4 · 3.1. Structural and morphological characterization · Fig. 2b-e
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag 3d3/2 binding energyapproximately 373.39 eVText
Rounded Reported
4 · 3.1. Structural and morphological characterization · Fig. 2d
Ag 3d5/2 binding energyapproximately 367.38 eVText
Rounded Reported
4 · 3.1. Structural and morphological characterization · Fig. 2d
Zn 2p1/2 binding energyapproximately 1044.31 eVText
Rounded Reported
4 · 3.1. Structural and morphological characterization · Fig. 2c
Zn 2p3/2 binding energyapproximately 1021.29 eVText
Rounded Reported
4 · 3.1. Structural and morphological characterization · Fig. 2c

XPS peak table and atomic composition

ZIF-8 · Powder

ZIF-8 XPS composition from SI Table S1; columns Peak BE, FWHM, Area(P) CPS.eV and Atomic %.

Context
pristine ZIF-8 control
Measurement source
4 · Table S1 · Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
C1s atomic percentage59 %SI Table
Exact Reported
4 · Table S1 · Table S1
N1s atomic percentage25.23 %SI Table
Exact Reported
4 · Table S1 · Table S1
O1s atomic percentage5.74 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p atomic percentage10.04 %SI Table
Exact Reported
4 · Table S1 · Table S1
Zn2p peak binding energy1021.46 eVSI Table
Exact Reported
4 · Table S1 · Table S1