Measurement evidence
Mechanistic Insight into the Formation and Deposition of Conductive, Layered Metal-Organic Framework Nanocrystals · Ambrogi E.K., Damacet P., Stolz R.M. et al. · ACS Nano · 2025 · 1383-1395
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
homogeneous DMF/water air plus H2O2 Ni3(HHTP)2, 85 C · Powder
background-corrected/normalised and raw traces compared with simulated ABAB pattern
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| ABAB/intercalated-layer PXRD assignment | characteristic Ni3(HHTP)2 peaks including (100) and intercalated-layer (002)/(31-1-) region | — | — | Qualitative Qualitative | p005 / journal page 1387 · Impact of Oxidants · Figure 1; Figure S7 |
heterogeneous water bubbled-air Ni3(HHTP)2, 85 C · Powder
background-corrected/normalised and raw traces compared with simulated ABAB pattern
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| ABAB/intercalated-layer PXRD assignmentMarked as a best value within this paper | characteristic Ni3(HHTP)2 peaks including (100) and intercalated-layer (002)/(31-1-) region | — | — | Qualitative Qualitative | p005 / journal page 1387 · Impact of Oxidants · Figure 1; Figure S7 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 85 C · Powder
background-corrected/normalised and raw traces compared with simulated ABAB pattern
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| ABAB/intercalated-layer PXRD assignmentMarked as a best value within this paper | characteristic Ni3(HHTP)2 peaks including (100) and intercalated-layer (002)/(31-1-) region | — | — | Qualitative Qualitative | p005 / journal page 1387 · Impact of Oxidants · Figure 1; Figure S7 |
| simulated PXRD peak (002)/(300)/(31-1-)/(102) overlapping region | 13.86 degrees 2theta; relative intensity 12% | — | — | SI Table Exact Reported | S8 · Table S1 · Table S1 |
| simulated PXRD peak (004) | 26.85 degrees 2theta; relative intensity 7.2% | — | — | SI Table Exact Reported | S8 · Table S1 · Table S1 |
| simulated PXRD peak (104) | 27.21 degrees 2theta; relative intensity 5.8% | — | — | SI Table Exact Reported | S8 · Table S1 · Table S1 |
| simulated PXRD peak (100) | 4.61 degrees 2theta; relative intensity 100% | — | — | SI Table Exact Reported | S8 · Table S1 · Table S1 |
homogeneous DMF/water N2 plus H2O2 Ni3(HHTP)2, 85 C · Powder
background-corrected/normalised and raw traces compared with simulated ABAB pattern
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| ABAB/intercalated-layer PXRD assignment | characteristic Ni3(HHTP)2 peaks including (100) and intercalated-layer (002)/(31-1-) region | — | — | Qualitative Qualitative | p005 / journal page 1387 · Impact of Oxidants · Figure 1; Figure S7 |
homogeneous DMF/water bubbled-N2 Ni3(HHTP)2, 85 C · Powder
background-corrected/normalised and raw traces compared with simulated ABAB pattern
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| ABAB/intercalated-layer PXRD assignment | characteristic Ni3(HHTP)2 peaks including (100) and intercalated-layer (002)/(31-1-) region | — | — | Qualitative Qualitative | p005 / journal page 1387 · Impact of Oxidants · Figure 1; Figure S7 |