Measurement evidence
Mechanistic Insight into the Formation and Deposition of Conductive, Layered Metal-Organic Framework Nanocrystals · Ambrogi E.K., Damacet P., Stolz R.M. et al. · ACS Nano · 2025 · 1383-1395
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
ATR air bubbled 1 mL/min Ni3(HHTP)2 · Thin Film
air-flow series products
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 233 +/- 84 nm | — | +/- 84 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
| average particle width | 57 +/- 15 nm | — | +/- 15 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
ATR air bubbled 2 mL/min Ni3(HHTP)2 · Thin Film
air-flow series products
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 268 +/- 98 nm | — | +/- 98 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
| average particle width | 59 +/- 14 nm | — | +/- 14 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
ATR air bubbled 4 mL/min Ni3(HHTP)2 · Thin Film
air-flow series products
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 172 +/- 53 nm | — | +/- 53 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
| average particle width | 79 +/- 21 nm | — | +/- 21 nm | SI Table Rounded Reported | S42 · Table S16 · Table S16 |
ATR in situ air-bubbled Ni3(HHTP)2, room temperature · Thin Film
MOF collected from in situ growth experiment
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 98 +/- 38 nm | — | +/- 38 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
| average particle width | 25 +/- 6 nm | — | +/- 6 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
ATR air-diffusion port-out Ni3(HHTP)2, room temperature · Thin Film
MOF collected from in situ growth experiment
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 275 +/- 125 nm | — | +/- 125 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
| average particle width | 43 +/- 11 nm | — | +/- 11 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
ATR air plus 50 uL 6% H2O2 Ni3(HHTP)2, room temperature · Thin Film
MOF collected from in situ growth experiment
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 1200 +/- 900 nm | — | +/- 900 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
| average particle width | 880 +/- 640 nm | — | +/- 640 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
ATR nitrogen-control Ni3(HHTP)2 attempt, room temperature · Thin Film
MOF collected from in situ growth experiment
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 62 +/- 31 nm | — | +/- 31 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
| average particle width | 37 +/- 19 nm | — | +/- 19 nm | SI Table Rounded Reported | S32 · Table S9 · Table S9 |
homogeneous DMF/water air plus H2O2 Ni3(HHTP)2, 85 C · Powder
atomic composition of bulk synthesis sample
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C 1s atomic composition | 55.75% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| Ni 2p atomic composition | 8.56% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| O 1s atomic composition | 35.69% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
heterogeneous water bubbled-air Ni3(HHTP)2, 85 C · Powder
atomic composition of bulk synthesis sample
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C 1s atomic composition | 64.76% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| Ni 2p atomic composition | 8.2% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| O 1s atomic composition | 27.03% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 85 C · Powder
atomic composition of bulk synthesis sample
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C 1s atomic composition | 68.7% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| Ni 2p atomic composition | 6.64% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| O 1s atomic composition | 24.65% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
homogeneous DMF/water N2 plus H2O2 Ni3(HHTP)2, 85 C · Powder
atomic composition of bulk synthesis sample
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C 1s atomic composition | 63.07% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| Ni 2p atomic composition | 8.15% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| O 1s atomic composition | 28.79% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
homogeneous DMF/water bubbled-N2 Ni3(HHTP)2, 85 C · Powder
atomic composition of bulk synthesis sample
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C 1s atomic composition | 68.6% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| Ni 2p atomic composition | 5.9% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
| O 1s atomic composition | 25.51% | — | — | SI Table Exact Reported | S21 · Table S6 · Table S6 |
homogeneous DMF/water air plus H2O2 Ni3(HHTP)2, 85 C · Powder
bulk synthesis products imaged by SEM
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 1700 +/- 1400 nm | — | +/- 1400 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
| average particle width | 1400 +/- 1300 nm | — | +/- 1300 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
heterogeneous water bubbled-air Ni3(HHTP)2, 85 C · Powder
bulk synthesis products imaged by SEM
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 249 +/- 223 nm | — | +/- 223 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
| average particle width | 58 +/- 34 nm | — | +/- 34 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 85 C · Powder
bulk synthesis products imaged by SEM
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 562 +/- 434 nm | — | +/- 434 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
| average particle width | 101 +/- 52 nm | — | +/- 52 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
homogeneous DMF/water N2 plus H2O2 Ni3(HHTP)2, 85 C · Powder
bulk synthesis products imaged by SEM
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 116 +/- 93 nm | — | +/- 93 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
| average particle width | 99 +/- 96 nm | — | +/- 96 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
homogeneous DMF/water bubbled-N2 Ni3(HHTP)2, 85 C · Powder
bulk synthesis products imaged by SEM
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| average particle length | 39 +/- 16 nm | — | +/- 16 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
| average particle width | 36 +/- 12 nm | — | +/- 12 nm | SI Table Rounded Reported | S15 · Table S4 · Table S4 |
ATR gradual 10 eq H2O2 over 2 h Ni3(HHTP)2 · Thin Film
gradual-addition rods
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| gradual-addition rods length | 192 +/- 75 nm | — | +/- 75 nm | SI Table Rounded Reported | S39 · Table S14 · Table S14 |
| gradual-addition rods width | 57 +/- 14 nm | — | +/- 14 nm | SI Table Rounded Reported | S39 · Table S14 · Table S14 |
ATR gradual 10 eq H2O2 over 4 h Ni3(HHTP)2 · Thin Film
gradual-addition rods
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| gradual-addition rods length | 170 +/- 77 nm | — | +/- 77 nm | SI Table Rounded Reported | S39 · Table S14 · Table S14 |
| gradual-addition rods width | 46 +/- 13 nm | — | +/- 13 nm | SI Table Rounded Reported | S39 · Table S14 · Table S14 |
ATR 1 eq H2O2 Ni3(HHTP)2 · Thin Film
aggregates
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| aggregates length | 1600 +/- 600 nm | — | +/- 600 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
| aggregates width | 1200 +/- 700 nm | — | +/- 700 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
ATR 1 eq H2O2 Ni3(HHTP)2 · Thin Film
nanorods
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| nanorods length | 64 +/- 16 nm | — | +/- 16 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
| nanorods width | 17 +/- 3 nm | — | +/- 3 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
ATR 3 eq H2O2 Ni3(HHTP)2 · Thin Film
aggregates
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| aggregates length | 600 +/- 500 nm | — | +/- 500 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
| aggregates width | 500 +/- 400 nm | — | +/- 400 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
ATR 3 eq H2O2 Ni3(HHTP)2 · Thin Film
nanorods
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| nanorods length | 79 +/- 20 nm | — | +/- 20 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
| nanorods width | 20 +/- 7 nm | — | +/- 7 nm | SI Table Rounded Reported | S38 · Table S12 · Table S12 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 22 C · Powder
bubbled-air synthesis at 22 C for 18 h
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| rod diameter | 43 +/- 11 nm | — | +/- 11 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |
| rod length | 275 +/- 125 nm | — | +/- 125 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 40 C · Powder
bubbled-air synthesis at 40 C for 18 h
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| rod diameter | 75 +/- 27 nm | — | +/- 27 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |
| rod lengthMarked as a best value within this paper | 587 +/- 229 nm | — | +/- 229 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |
homogeneous DMF/water bubbled-air Ni3(HHTP)2, 85 C · Powder
bubbled-air synthesis at 85 C for 18 h
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| rod diameter | 101 +/- 52 nm | — | +/- 52 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |
| rod length | 562 +/- 434 nm | — | +/- 434 nm | SI Table Rounded Reported | S22 · Table S7 · Table S7 |