cMOF Evidence Base
Other — New coordination polymers of 1,4-bis(2′-hydroxyphenylazomethine) phenylene

Measurement evidence

Other

New coordination polymers of 1,4-bis(2′-hydroxyphenylazomethine) phenylene · Hassan M.K., Abd-Alla M.A., Hasan R.M. · Journal of Macromolecular Science: Part A - Chemistry · 1990 · 1501-1512

17 measurement groups · 76 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Elemental analysis

Bulk elemental and compositional analysis

Cr-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourDark brown——Table
Qualitative		1506 · Results · Table 1
calculated metal content12.38%——Table
Exact Reported		1506 · Results · Table 1
found metal content12.51%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight419.82——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Cr-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 150 deg C3.5 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 200 deg C7 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C18 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C30 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C65 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C77 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C80 wt%——Table
Exact Reported		1509 · Results · Table 3

Inherent viscosity

Cr-BHPAP polychelate powder · Powder

0.5 g/100 mL DMF polymer solution; Ubbelohde suspended-level viscometer; 30 deg C.

Context
pristine coordination polymer
Measurement source
1503-1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
inherent viscosity0.5 dL/g——Table
Exact Reported		1506 · Results · Table 1

Elemental analysis

Bulk elemental and compositional analysis

Cu-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourDark green——Table
Qualitative		1506 · Results · Table 1
calculated metal content16.81%——Table
Exact Reported		1506 · Results · Table 1
found metal content16.96%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight377.69——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Cu-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 200 deg C8.5 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C15 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C38 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C55 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C65 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C83 wt%——Table
Exact Reported		1509 · Results · Table 3

Inherent viscosity

Cu-BHPAP polychelate powder · Powder

0.5 g/100 mL DMF polymer solution; Ubbelohde suspended-level viscometer; 30 deg C.

Context
pristine coordination polymer
Measurement source
1503-1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
inherent viscosity0.38 dL/g——Table
Exact Reported		1506 · Results · Table 1

Elemental analysis

Bulk elemental and compositional analysis

Fe-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourDark brown——Table
Qualitative		1506 · Results · Table 1
calculated metal content13.18%——Table
Exact Reported		1506 · Results · Table 1
found metal content13.27%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight423.69——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Fe-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 150 deg C4.5 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 200 deg C9 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C25 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C32 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C62 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C77 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C82 wt%——Table
Exact Reported		1509 · Results · Table 3

Inherent viscosity

Fe-BHPAP polychelate powder · Powder

0.5 g/100 mL DMF polymer solution; Ubbelohde suspended-level viscometer; 30 deg C.

Context
pristine coordination polymer
Measurement source
1503-1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
inherent viscosity0.42 dL/g——Table
Exact Reported		1506 · Results · Table 1

Elemental analysis

Bulk elemental and compositional analysis

Mn-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourBlack——Table
Qualitative		1506 · Results · Table 1
calculated metal content13.55%——Table
Exact Reported		1506 · Results · Table 1
found metal content13.6%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight405.32——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Mn-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 150 deg C8 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 200 deg C10 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C20 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C35 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C60 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C72 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C83 wt%——Table
Exact Reported		1509 · Results · Table 3

Elemental analysis

Bulk elemental and compositional analysis

Ni-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourBlack——Table
Qualitative		1506 · Results · Table 1
calculated metal content14.35%——Table
Exact Reported		1506 · Results · Table 1
found metal content14.22%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight409.09——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Ni-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 150 deg C2.5 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 200 deg C9 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C17.5 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C30 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C59 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C65 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C84 wt%——Table
Exact Reported		1509 · Results · Table 3

Inherent viscosity

Ni-BHPAP polychelate powder · Powder

0.5 g/100 mL DMF polymer solution; Ubbelohde suspended-level viscometer; 30 deg C.

Context
pristine coordination polymer
Measurement source
1503-1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
inherent viscosity0.61 dL/g——Table
Exact Reported		1506 · Results · Table 1

Elemental analysis

Bulk elemental and compositional analysis

Ti-BHPAP polychelate powder · Powder

C/H/N by Perkin-Elmer 240 C; chlorine determined by departmental analytical unit.

Context
pristine coordination polymer
Measurement source
1503,1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported colourBrown——Table
Qualitative		1506 · Results · Table 1
calculated metal content11.52%——Table
Exact Reported		1506 · Results · Table 1
found metal content11.64%——Table
Exact Reported		1506 · Results · Table 1
melting/decomposition entry>360 deg C——Table
Approximate		1506 · Results · Table 1
repeat unit molecular weight415.72——Table
Exact Reported		1506 · Results · Table 1

Thermogravimetric analysis

Thermogravimetric analysis

Ti-BHPAP polychelate powder · Powder

Du Pont thermal analysers; air; heating rate 10 deg C/min; data reported up to 700 deg C in Table 3 and text discusses 750 deg C.

Context
pristine coordination polymer
Measurement source
1503,1509-1511 · Measurements; Results · Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
weight loss at 150 deg C7 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 200 deg C10 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 300 deg C22 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 400 deg C35 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 500 deg C60 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 600 deg C68 wt%——Table
Exact Reported		1509 · Results · Table 3
weight loss at 700 deg C85 wt%——Table
Exact Reported		1509 · Results · Table 3

Inherent viscosity

Ti-BHPAP polychelate powder · Powder

0.5 g/100 mL DMF polymer solution; Ubbelohde suspended-level viscometer; 30 deg C.

Context
pristine coordination polymer
Measurement source
1503-1506 · Measurements; Results · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
inherent viscosity0.34 dL/g——Table
Exact Reported		1506 · Results · Table 1