Diffraction Structure — Highly Selective CO2 Electroreduction to CH4 by In Situ Generated Cu2O Single-Type Sites on a Conductive MOF: Stabilizing Key Intermediates with Hydrogen Bonding

Measurement evidence

Diffraction Structure

Highly Selective CO2 Electroreduction to CH4 by In Situ Generated Cu2O Single-Type Sites on a Conductive MOF: Stabilizing Key Intermediates with Hydrogen Bonding · Yi J.-D., Xie R., Xie Z.-L. et al. · Angewandte Chemie - International Edition · 2020 · 23641-23648

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction (PXRD)

X-ray diffraction and scattering

Cu2O@CuHHTP, -1.2 V 30 min · Electrode

Cu K alpha radiation, lambda = 0.154 nm

Geometry: Miniflex 600 diffractometer
Context: pristine CuHHTP and electroreduced composite
Measurement source: p002 / SI p1 · Characterization · Figure 1b; Figure S12

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Other copper phases in target PXRD	No Cu, CuO or Cu(OH)2 peaks observed	—	—	Text Qualitative	p003 / 23643 · Figure 1b
Cu2O(111) PXRD peak in Cu2O@CuHHTP	new peak centred at 36.5 degrees	—	—	Text Rounded Reported	p003 / 23643 · Figure 1b