Diffraction Structure — Understanding Solvothermal Growth of Metal-Organic Framework Colloids for CO2Capture Applications

18 measurement groups · 18 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu0.3BTC-100-8 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	24.1 +/- 0.2	—	+/- 0.2 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-100-14 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	31.4 +/- 0.4	—	+/- 0.4 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-100-20 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	32.4 +/- 0.3	—	+/- 0.3 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-100-3 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	25.5 +/- 1.1	—	+/- 1.1 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-100-5 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	28.8 +/- 1.6	—	+/- 1.6 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-100-8 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	29.7 +/- 1.1	—	+/- 1.1 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-120-14 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	32.4 +/- 0.3	—	+/- 0.3 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-120-20 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	35.1 +/- 0.6	—	+/- 0.6 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-120-3 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	27.5 +/- 0.1	—	+/- 0.1 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-120-5 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	30.8 +/- 1.3	—	+/- 1.3 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-120-8 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	32.2 +/- 0.1	—	+/- 0.1 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-80-14 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	26.9 +/- 2.1	—	+/- 2.1 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-80-20 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	28.7 +/- 1.7	—	+/- 1.7 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-80-3 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	21.8 +/- 1.6	—	+/- 1.6 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-80-5 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	22.3 +/- 1.6	—	+/- 1.6 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu1BTC-80-8 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	24.7 +/- 0.3	—	+/- 0.3 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD), Cu Kalpha radiation

X-ray diffraction and scattering

1Cu3BTC-100-8 · Powder

D2 Phaser diffractometer; Cu Kalpha radiation, 30 kV, 10 mA, 2theta 5-50 deg, scan rate 3.0 deg/min; crystallite size calculated from the 11.6 deg (222) HKUST-1 peak by Scherrer equation.

Context: pristine Cu-MOF colloid
Measurement source: 4417-4418 · Materials and Methods; Results and Discussion · Figure 2; Table 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	32.0 +/- 2.4	—	+/- 2.4 nm	Table Exact Reported	4418 · Results and Discussion · Table 2

Powder X-ray diffraction (XRD)

X-ray diffraction and scattering

3Cu1BTC-100-8 · Powder

SI Section 7 copper-source variant; XRD pattern in Figure S13c with similar dc value reported as a range.

Context: pristine Cu-MOF colloid
Measurement source: S16 · Material characterization of the Cu-MOF prepared by a different amount of copper · Figure S13c

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Scherrer crystallite size dc	28-30	—	range 28-30 nm	Text Range	S16 · Material characterization of the Cu-MOF prepared by a different amount of copper · Figure S13c