Partial recipeSource: Main
Route 1: Solvothermal
p003 / journal p.951 · Results and discussions · Table 2
Metal precursorsCoCl2 or FeCl2
Linker precursorsNa2AQDS
Solventswater and n-BuOH, molar composition equivalent to optimised rare-earth mixture
Additivesnone reported
Atmospherenot specified
Temperature180
Time18
Oxidant / reductantnone; AQDS remains dianionic/non-radical
Work-upnot described
Activationnone reported
Scalability contextControl products show the same structural type but no radical formation.
Show 4 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | CoCl2 | not reported · equivalent to optimised rare-earth mixture | p003 / journal p.951 · Results and discussions · Table 2 |
| Metal Source | FeCl2 | not reported · equivalent to optimised rare-earth mixture | p003 / journal p.951 · Results and discussions · Table 2 |
| Linker | Na2AQDS | not reported · equivalent to optimised rare-earth mixture | p003 / journal p.951 · Results and discussions · Table 2 |
| Solvent | water/n-BuOH | not reported · equivalent to optimised rare-earth mixture | p003 / journal p.951 · Results and discussions · Table 2 |