Complete recipeSource: Main
Route 1: Solvothermal
2-3 · 2.3 Synthesis of Cu-MOFs/EGP
Metal precursorsCu(NO3)2.2.5H2O, 156.8 mg
Linker precursors3-amino-5-mercapto-1,2,4-triazole (AMTA), 104.5 mg
Solvents20 mL DMF/ethanol solvent mixture, V_DMF:V_ethanol = 1:1
Additivesexfoliated graphite paper substrate placed in the autoclave
Atmospherenot reported
Temperature120
Time12
Substrate orientationpiece of EGP placed in advance in a 40 mL Teflon-lined autoclave
Work-upWashed three times with DMF and ethanol separately.
ActivationDried overnight under vacuum at 120 deg C.
Scalability context40 mL autoclave with one EGP piece; no yield or scale-up discussion.
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Cu(NO3)2.2.5H2O | 156.8 mg | 2-3 · 2.3 Synthesis of Cu-MOFs/EGP |
| Linker | 3-amino-5-mercapto-1,2,4-triazole (AMTA) | 104.5 mg | 2-3 · 2.3 Synthesis of Cu-MOFs/EGP |
| Solvent | N,N-dimethylformamide (DMF) | part of 20 mL DMF/ethanol mixture · V_DMF:V_ethanol = 1:1 | 2-3 · 2.3 Synthesis of Cu-MOFs/EGP |
| Solvent | ethanol | part of 20 mL DMF/ethanol mixture · V_DMF:V_ethanol = 1:1 | 2-3 · 2.3 Synthesis of Cu-MOFs/EGP |
| Other | exfoliated graphite paper (EGP) | one piece | 2-3 · 2.3 Synthesis of Cu-MOFs/EGP |