Diffraction Structure — Two dimensional Conjugated Metal–Organic Frameworks with Multiple Redox-Active Sites towards High-Performance Sodium-Ion Battery

Measurement evidence

Diffraction Structure

Two dimensional Conjugated Metal–Organic Frameworks with Multiple Redox-Active Sites towards High-Performance Sodium-Ion Battery · Qi M., Cheng L., Zhang X. et al. · Advanced Science · 2025 · 2503369

4 measurement groups · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD with Pawley refinement

Cu-DDQP black powder · Powder

PXRD experimental/refined/calculated patterns in Figure 2b.

Atmosphere
ambient
Geometry
powder
Context
pristine Cu-DDQP powder
Measurement source
4 · Results and Discussion · Figure 2b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pawley RpRp = 2.57%Figure Axis
Rounded Reported
4 · Results · Figure 2b
Pawley RwpRwp = 3.39%Figure Axis
Rounded Reported
4 · Results · Figure 2b
AA stacking d-spacing3.21 AText
Rounded Reported
4 · Results · Figure 1b-d

PXRD with Pawley refinement

Cu-TBPQ black powder · Powder

PXRD experimental/refined/calculated patterns in Figure 2a.

Atmosphere
ambient
Geometry
powder
Context
pristine Cu-TBPQ powder
Measurement source
4 · Results and Discussion · Figure 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pawley RpRp = 5.29%Figure Axis
Rounded Reported
4 · Results · Figure 2a
Pawley RwpRwp = 7.71%Figure Axis
Rounded Reported
4 · Results · Figure 2a
AA stacking d-spacing3.49 AText
Rounded Reported
4 · Results · Figure 1b-d

PXRD with Pawley refinement

Cu-TTPQ black powder · Powder

PXRD compared with simulated stacking models; Cu target tube.

Atmosphere
ambient
Geometry
powder
Context
pristine Cu-TTPQ powder
Measurement source
4 · Results and Discussion · Figure 2c; Figure S12
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pawley cell aa = 19.22 AText
Rounded Reported
4 · Results · Figure 2c
Pawley cell bb = 19.21 AText
Rounded Reported
4 · Results · Figure 2c
Pawley cell cc = 3.16 AText
Rounded Reported
4 · Results · Figure 2c
Pawley gamma anglegamma = 111.2 degText
Rounded Reported
4 · Results · Figure 2c
Pawley RpRp = 2.61%Text
Exact Reported
4 · Results · Figure 2c
Pawley RwpRwp = 3.42%Text
Exact Reported
4 · Results · Figure 2c

solvent stability PXRD

Cu-TTPQ black powder · Powder

Cu-TTPQ immersed in H2O, THF, acetone, DMF, 1 M AcOH and 1 M NaOH for five days; PXRD after exposure.

Geometry
powder
Context
pristine Cu-TTPQ powder
Measurement source
S22 · Section 11 Chemical Stability Tests · Figure S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Solvent stabilityPXRD retained after five days in H2O, THF, acetone, DMF, 1 M AcOH and 1 M NaOHQualitative
Qualitative
S22 · Section 11 · Figure S20