cMOF Evidence Base
Diffraction Structure — A simplistic approach for the synthesis of Covalent Organic Frameworks(COFs) comprising of tetrafunctionalized porphyrin and polyoxometalates to uncover catalytic applications

Measurement evidence

Diffraction Structure

A simplistic approach for the synthesis of Covalent Organic Frameworks(COFs) comprising of tetrafunctionalized porphyrin and polyoxometalates to uncover catalytic applications · Rani S., Tariq M., Bhatti M.H. et al. · Optical Materials · 2023 · 113672

2 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD with Williamson-Hall analysis; SEM morphology

X-ray diffraction and scatteringScanning electron microscopyHall-effect measurements

P@Cu-AndCOF bulk solid · Powder

Bulk P@Cu-AndCOF powder/solid.

Context
Pristine bulk framework.
Measurement source
main p.7-8 · 3. Results and discussion · Figures 5-7; Tables S5-S7 referenced
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Williamson-Hall crystal size16.7053012 nm in SI Table S6; main text states 27.34792899 nm——SI Table
Exact Reported		SI p.8 · Table S6 · Table S6
PXRD crystallinity percentage72%——SI Table
Exact Reported		SI p.9 · Table S7 · Table S7
PXRD Williamson-Hall peak table2theta/FWHL/betaCosTheta/4SinTheta rows: 7.67225/0.488/0.008494/0.267477; 12.6305/1.60717/0.027866/0.439773; 14.494/0.49905/0.008636/0.504334; 19.43936/0.44727/0.00769/0.674973; 21.18502/0.8802/0.015093/0.734923; 26.12801/64.95607/1.103825/0.903707; 29.91882/0.52735/0.008888/1.032027; 32.96566/0.39997/0.006691/1.134353; 45.41607/10.09107/0.162401/1.5434——SI Table
Exact Reported		SI p.8 · Table S6 · Table S6
SEM morphologyregular distributed crystalline polymeric form; rod-like morphology——Qualitative
Qualitative		main p.8 · 3. Results and discussion · Figure 7
Williamson-Hall strain0.3874 in SI Table S6; main text states -0.80557——SI Table
Exact Reported		SI p.8 · Table S6 · Table S6

PXRD with Williamson-Hall analysis; SEM morphology

X-ray diffraction and scatteringScanning electron microscopyHall-effect measurements

P@Ni-AndCOF bulk solid · Powder

Bulk P@Ni-AndCOF powder/solid.

Context
Pristine bulk framework.
Measurement source
main p.7-8 · 3. Results and discussion · Figures 5-7; Tables S5-S7 referenced
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Williamson-Hall crystal size6.057405 nm——SI Table
Exact Reported		SI p.7-8 · Table S5 · Table S5
PXRD crystallinity percentage54%——SI Table
Exact Reported		SI p.9 · Table S7 · Table S7
PXRD Williamson-Hall peak table2theta/FWHL/betaCosTheta/4SinTheta rows: 5.76528/1.02499/-0.01728/0.201059; 7.43162/0.54/-0.00791/0.259099; 10.63037/0.49689/0.004914/0.370351; 12.69867/0.37559/0.006538/0.442137; 21.44862/0.49178/-0.0023/0.743961; 23.70674/0.37559/0.004956/0.82122; 35.70252/0.36243/0.003425/1.225587; 42.20432/0.39053/-0.00429/1.439431; 49.05067/0.4543/0.006507/1.659593——SI Table
Exact Reported		SI p.7-8 · Table S5 · Table S5
SEM morphologyregular distributed crystalline polymeric form; rod-like morphology——Qualitative
Qualitative		main p.8 · 3. Results and discussion · Figure 7
Williamson-Hall strain-0.00281——SI Table
Exact Reported		SI p.7-8 · Table S5 · Table S5