Diffraction Structure — Effect of solvent on the perovskite thin film morphology and crystallinity

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

DMF-derived MAPbI3 film on mesoporous TiO2 · Thin Film

DMF-derived film after 100 C heating for 0.5 h in glovebox.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
DMF intermediate conversion after annealing	low-angle MOF peaks disappear and perovskite peaks strengthen after 100 C annealing	—	—	Text Qualitative	038403-5 · 3.2 · Figure 5(a)
MAPbI3 XRD (110) peak	14.17 degrees 2theta	—	—	Text Exact Reported	038403-5 · 3.2 · Figure 5(a)
MAPbI3 XRD (220) peak	28.49 degrees 2theta	—	—	Text Exact Reported	038403-5 · 3.2 · Figure 5(a)
MAPbI3 XRD (330) peak	43.27 degrees 2theta	—	—	Text Exact Reported	038403-5 · 3.2 · Figure 5(a)

unannealed DMF-derived PbI2-MAI-DMF layered MOF film · Thin Film

Unheated DMF-derived spin-coated film; samples prepared in glovebox, sealed in quartz box, measured within 10 min, RH below 40%.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
low-angle peaks of PbI2-MAI-DMF intermediate	three strong peaks before 10 degrees 2theta	—	<10 degrees; individual peak positions not tabulated	Text Range	038403-5 · 3.2 · Figure 5(a)

GBL-derived MAPbI3 film on mesoporous TiO2 · Thin Film

GBL-derived spin-coated film after annealing.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
GBL annealed film phase conversionMarked as a best value within this paper	peak positions and relative intensities indicate complete conversion to perovskite	—	—	Text Qualitative	038403-6 · 3.2 · Figure 5(c)