Microscopy Morphology — Effect of solvent on the perovskite thin film morphology and crystallinity

4 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

DMF-derived MAPbI3 film on copper grid · Thin Film

High-resolution imaging of film prepared directly on copper grid to minimise water-vapour effects.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HRTEM defect observation	ordered crystallographic orientation but clear dislocation defects	—	—	Text Qualitative	038403-4 · 3.1 · Figure 2(a)

GBL-derived MAPbI3 film on copper grid · Thin Film

High-resolution imaging of film prepared directly on copper grid to minimise water-vapour effects.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HRTEM defect observationMarked as a best value within this paper	high crystallinity and no obvious defects in the field of view	—	—	Text Qualitative	038403-4 · 3.1 · Figure 2(b)

DMF-derived MAPbI3 film on mesoporous TiO2 · Thin Film

Surface and cross-section imaging of DMF-derived film on mesoporous TiO2.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
DMF strip-like crystal length	3-5 um	—	range 3-5 um	Text Range	038403-2 · 3.1 · Figure 1(a,b)
DMF strip-like crystal width	0.5-1 um	—	range 0.5-1 um	Text Range	038403-2 · 3.1 · Figure 1(a,b)
mesoporous TiO2 filling quality	poor filling; many exposed mesoporous TiO2 regions and obvious gaps	—	—	Text Qualitative	038403-3 · 3.1 · Figure 1(c)
DMF ribbon-like crystal thickness	about 200 nm	—	about	Text Approximate	038403-3 · 3.1 · Figure 1(c)

GBL-derived MAPbI3 film on mesoporous TiO2 · Thin Film

Surface and cross-section imaging of GBL-derived film on mesoporous TiO2.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
GBL capping layer thicknessMarked as a best value within this paper	about 200 nm	—	about	Text Approximate	038403-4 · 3.1 · Figure 1(f)
mesoporous TiO2 filling qualityMarked as a best value within this paper	dense filling and good contact between perovskite and TiO2 particles	—	—	Text Qualitative	038403-4 · 3.1 · Figure 1(f)