Microscopy Morphology — A Triptycene-Based 2D MOF with Vertically Extended Structure for Improving the Electrocatalytic Performance of CO2 to Methane

Measurement evidence

Microscopy Morphology

A Triptycene-Based 2D MOF with Vertically Extended Structure for Improving the Electrocatalytic Performance of CO2 to Methane · Lv J., Li W., Li J. et al. · Angewandte Chemie - International Edition · 2023 · e202217958

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

AFM, SEM, FT-IR, XPS, HR-TEM, SAED after dry grinding

Infrared spectroscopy X-ray photoelectron spectroscopy Scanning electron microscopy Transmission electron microscopy Atomic force microscopy

exfoliated 2D-vc-MOF(Cu) nanosheets · Nanosheet

Exfoliated nanosheets characterised for lateral size, thickness, chemical retention, and diffraction.

Context: exfoliated pristine framework nanosheets
Measurement source: 3 · The Synthesis and Characterization of 2D-vc-MOF(Cu) · Figures S17-S22; Tables S6-S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Exfoliated nanosheet lateral size	several micrometers	—	—	Text Approximate	3 · The Synthesis and Characterization of 2D-vc-MOF(Cu) · Figure S18
Exfoliated nanosheet mean thickness	about 7 nm, corresponding to about 10 layers	—	—	Text Approximate	3 · The Synthesis and Characterization of 2D-vc-MOF(Cu) · Figure S19

SEM, TEM, HR-TEM

Scanning electron microscopy Transmission electron microscopy

2D-vc-MOF(Cu) blue-black powder · Powder

Morphology and lattice imaging of pristine powder.

Context: pristine target MOF
Measurement source: 3 · The Synthesis and Characterization of 2D-vc-MOF(Cu) · Figures S11-S13

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source