Diffraction Structure — Synthesis, characterization, and solid state electrical conductivity of coordination polymers with copper and zinc

Measurement evidence

Diffraction Structure

Synthesis, characterization, and solid state electrical conductivity of coordination polymers with copper and zinc · Prasad R.L., Kushwaha A. · Journal of Coordination Chemistry · 2012 · 4230-4244

6 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 2 compressed pellet · Pellet

Room-temperature PXRD with Cu-Kalpha radiation, lambda = 1.541836 A.

Temperature: room temperature
Geometry: powder sample
Context: monometallic control
Measurement source: p004 / 4232 · 2.3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 3 compressed pellet · Pellet

Room-temperature PXRD with Cu-Kalpha radiation.

Temperature: room temperature
Geometry: powder sample
Context: monometallic control
Measurement source: SI p12 · Figure S6(a) · Figure S6(a)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 4 compressed pellet · Pellet

Room-temperature PXRD compared with complexes 2, 3 and their equimolar mixture.

Temperature: room temperature
Geometry: powder sample
Context: mixed-metal target
Measurement source: p006 / 4234 · 3.1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Complex 4 distinct PXRD lines between 12 and 40 deg 2theta	12 distinct lines	—	—	Text Exact Reported	p006 / 4234 · 3.1
Complex 4 phase identity	4 is neither 2 nor a mixture of 2 and 3; it has a new identity.	—	—	Text Qualitative	p006 / 4234 · 3.1

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 5 compressed pellet · Pellet

PXRD for complexes 2-6 and equimolar mixture of 2 and 3.

Temperature: room temperature
Geometry: powder sample
Context: mixed-metal target
Measurement source: p006 / 4234 · 3.1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Complex 5 distinct PXRD lines between 12 and 40 deg 2theta	17 distinct lines	—	—	Text Exact Reported	p006 / 4234 · 3.1

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 6 compressed pellet · Pellet

PXRD for complexes 2-6 and equimolar mixture of 2 and 3.

Temperature: room temperature
Geometry: powder sample
Context: mixed-metal target
Measurement source: p006 / 4234 · 3.1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Complex 6 distinct PXRD lines between 12 and 40 deg 2theta	28 distinct lines	—	—	Text Exact Reported	p006 / 4234 · 3.1

Powder X-ray diffraction

X-ray diffraction and scattering

Complex 7 compressed pellet · Pellet

PXRD pattern for 7 compared with 2, 3, 4 and dadb.

Temperature: room temperature
Geometry: powder sample
Context: mixed-metal target
Measurement source: SI p13 · Figure S6(b) · Figure S6(b)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source