Diffraction Structure — Tunable Capacitive Behavior in Metallopolymer-based Electrochromic Thin Film Supercapacitors

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

poly-Fe-L1 isolated metallopolymer powder · Powder

PXRD with Cu K-alpha radiation; FT-IR in KBr; Raman spectra; XPS with Al K-alpha; TGA in nitrogen at 10 degrees C/min

Atmosphere: nitrogen for TGA; otherwise ambient/solid-state as applicable
Context: pristine metallopolymer powder
Measurement source: p002-p004 · Materials and Methods; Synthesis and Characterization · Figures S1-S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD phase assignment	amorphous, with very modest molecular ordering in poly-Fe-L1	—	—	Text Qualitative	p004 · Synthesis and Characterization · Figure S2
TGA weight retained at 1000 degrees C	45.5 wt% retained at 1000 degrees C for poly-Fe-L1	—	—	Visual Estimate Rounded Reported	p012 · Supporting Figures · Figure S3
Fe2+ 3p3/2 binding energy	709 eV	—	—	Text Rounded Reported	p004 · Synthesis and Characterization · Figure S4

poly-Fe-L2 isolated metallopolymer powder · Powder

PXRD with Cu K-alpha radiation; FT-IR in KBr; Raman spectra; XPS with Al K-alpha; TGA in nitrogen at 10 degrees C/min

Atmosphere: nitrogen for TGA; otherwise ambient/solid-state as applicable
Context: pristine metallopolymer powder
Measurement source: p002-p004 · Materials and Methods; Synthesis and Characterization · Figures S1-S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TGA weight retained at 1000 degrees C	45.4 wt% retained at 1000 degrees C for poly-Fe-L2	—	—	Visual Estimate Rounded Reported	p012 · Supporting Figures · Figure S3

poly-Fe-L3 isolated metallopolymer powder · Powder

PXRD with Cu K-alpha radiation; FT-IR in KBr; Raman spectra; XPS with Al K-alpha; TGA in nitrogen at 10 degrees C/min

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TGA weight retained at 1000 degrees CMarked as a best value within this paper	48.9 wt% retained at 1000 degrees C for poly-Fe-L3	—	—	Visual Estimate Rounded Reported	p012 · Supporting Figures · Figure S3