Measurement evidence
Correlation in Structural Architecture toward Fabrication of Schottky Device with a Series of Pyrazine Appended Coordination Polymers · Bhunia S., Sahoo D., Dutta B. et al. · Inorganic Chemistry · 2023 · 20948-20960
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
As-synthesised crystals/powder of 1 · Powder
PXRD with Cu Kalpha radiation, 1.548 A, room temperature; TGA 30-800 C at 10 C/min under N2.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Thermal stability limit | stable up to nearly 267 C | — | — | Text Approximate | 20949 · Synthesis and Formulation · Figure S5 |
As-synthesised crystals/powder of 2 · Powder
PXRD with Cu Kalpha radiation, 1.548 A, room temperature; TGA 30-800 C at 10 C/min under N2.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Thermal stability limit | stable up to nearly 391 C | — | — | Text Approximate | 20949 · Synthesis and Formulation · Figure S5 |
As-synthesised crystals/powder of 3 · Powder
PXRD with Cu Kalpha radiation, 1.548 A, room temperature; TGA 30-800 C at 10 C/min under N2.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Thermal stability limitMarked as a best value within this paper | stable up to nearly 423 C | — | — | Text Approximate | 20949 · Synthesis and Formulation · Figure S5 |
As-synthesised crystals/powder of 1 · Powder
Mo-Kalpha radiation, lambda = 0.71073 A; 273(2) K; Bruker APEX-II CCD; SHELX-97 refinement.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Shortest reported pi-pi ring-centroid distance | 5.114(14) | — | (14) | SI Table Exact Reported | S12 · pi-pi interaction · Table S7 |
| Space group | P-1 | — | — | SI Table Exact Reported | S9 · Crystal data · Table S1 |
As-synthesised crystals/powder of 2 · Powder
Mo-Kalpha radiation, lambda = 0.71073 A; 273 K; Bruker APEX-II CCD; SHELX-97 refinement.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Shortest reported pi-pi ring-centroid distance | 4.31(18) | — | (18) | SI Table Exact Reported | S12 · pi-pi interaction · Table S7 |
| Space group | Ccca | — | — | SI Table Exact Reported | S10 · Crystal data · Table S3 |
As-synthesised crystals/powder of 3 · Powder
Mo-Kalpha radiation, lambda = 0.71073 A; 273(2) K; Bruker APEX-II CCD; SHELX-97 refinement.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Shortest reported pi-pi ring-centroid distanceMarked as a best value within this paper | 4.14(3) | — | (3) | SI Table Exact Reported | S12 · pi-pi interaction · Table S7 |
| Space group | P-1 | — | — | SI Table Exact Reported | S11 · Crystal data · Table S5 |