cMOF Evidence Base
Microscopy Morphology — sp-Carbon Incorporated Conductive Metal-Organic Framework as Photocathode for Photoelectrochemical Hydrogen Generation

Measurement evidence

Microscopy Morphology

sp-Carbon Incorporated Conductive Metal-Organic Framework as Photocathode for Photoelectrochemical Hydrogen Generation · Lu Y., Zhong H., Li J. et al. · Angewandte Chemie - International Edition · 2022 · e202208163

2 measurement groups · 1 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HRTEM and zero-loss filtered SAED

Transmission electron microscopy

as-synthesised Cu3HHAE2 powder/hexagonal rods · Powder

HRTEM of crystallite near (001) zone axis; elastically filtered SAED compared with simulated powder pattern.

Atmosphere
TEM vacuum
Geometry
tiny crystallite
Context
pristine crystallite
Measurement source
3 · Structure characterisation · Figure 2d,e
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

SEM

Scanning electron microscopy

as-synthesised Cu3HHAE2 powder/hexagonal rods · Powder

SEM images recorded on Zeiss Gemini S4500; Figure 1b and Figure S3.

Context
pristine powder morphology
Measurement source
2 · Results and discussion · Figure 1b; Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
hexagonal rod length1-5 um—rangeText
Range		2 · Results and discussion · Figure 1b; Figure S3