Porosity — sp-Carbon Incorporated Conductive Metal-Organic Framework as Photocathode for Photoelectrochemical Hydrogen Generation

Measurement evidence

Porosity

sp-Carbon Incorporated Conductive Metal-Organic Framework as Photocathode for Photoelectrochemical Hydrogen Generation · Lu Y., Zhong H., Li J. et al. · Angewandte Chemie - International Edition · 2022 · e202208163

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption/desorption isotherms and BET analysis

as-synthesised Cu3HHAE2 powder/hexagonal rods · Powder

N2 sorption at 77 K / 77.3 K; powder treated in supercritical CO2 dryer 4 h and activated at 90 deg C overnight / under dynamic vacuum.

Temperature
77
Atmosphere
N2
Context
activated pristine powder
Measurement source
2 · Porosity · Figure 1c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper801 m2 g-1Text
Exact Reported
2 · Porosity · Figure 1c
hexagonal channel/pore diameterabout 2.2 nmaboutText
Approximate
3 · Structure characterisation · Figure 2
average pore size from N2 isotherm fitting2.16 nmText
Exact Reported
2 · Porosity · Figure 1c
triangular pore diameter0.3 nmText
Rounded Reported
3 · Structure characterisation · Figure 2