Diffraction Structure — Operando Raman and ex situ characterization of an iron-based conductive MOF as a negative electrode in Li-ion batteries

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

synthesised Fe-HHTP powder · Powder

D-Max Rigaku Ru300 rotating anode; 3-50 degrees 2theta; 0.03 degree step; 1 s per step.

Geometry: powder
Context: pristine Fe-HHTP powder
Measurement source: 10 · 4.2 Powder and electrodes ex situ characterization techniques · Figure 1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD crystallinity	Weak PXRD pattern; low-crystalline material	—	—	Text Qualitative	2 · 2.1 MOF powder characterization · Figure 1a
PXRD weak reflection positions	approximately 9.3, 15.1, 16.5, 21.3, 25.7, 27.1 and 27.5 degrees 2theta	—	—	Text Approximate	2 · 2.1 MOF powder characterization · Figure 1a

Fresh and cycled Fe-HHTP composite electrodes stopped at 0.1 V or 3 V · Electrode

5-35 degrees 2theta; 0.03 degree step; 2 s per step for the fresh electrode.

Geometry: composite electrode
Context: fresh composite electrode before cycling
Measurement source: 10 · 4.2 Powder and electrodes ex situ characterization techniques · Figure S8

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Fresh electrode XRD structural information	no discernible peaks in fresh electrode XRD; structural changes with cycles cannot be obtained by XRD	—	—	Text Qualitative	9 · Figure S8 · Figure S8