Other — Operando Raman and ex situ characterization of an iron-based conductive MOF as a negative electrode in Li-ion batteries

Measurement evidence

Other

Operando Raman and ex situ characterization of an iron-based conductive MOF as a negative electrode in Li-ion batteries · Ciria-Ramos I., Neale A.R., Hardwick L.J. et al. · Dalton Transactions · 2025 · 9714-9725

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis (TGA)

Thermogravimetric analysis

synthesised Fe-HHTP powder · Powder

TA Instruments SDT 2960; room temperature to 700 C; 5 C min-1; air.

Atmosphere: air
Geometry: powder
Context: pristine Fe-HHTP powder
Measurement source: 10 · 4.2 Powder and electrodes ex situ characterization techniques · Figure S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Thermal decomposition endpoint	thermal decomposition until 475 C, probably leaving iron oxides	—	—	Text Rounded Reported	3 · 2.1 MOF powder characterization · Figure S5
Low-temperature mass loss	23% weight loss from room temperature to 240 C, assigned to DMF and H2O leaving the MOF structure	—	—	Text Rounded Reported	3 · 2.1 MOF powder characterization · Figure S5