powder X-ray diffraction
near-ideal Ni3(HITP)2 crystallite powder · Powder
PANalytical Empyrean Cu sealed tube, lambda = 1.544426 Angstrom, 40 kV, 40 mA; thin powder layer on roughened glass plate.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD phase assignment | matches simulated XRD and reported Ni3(HITP)2 | — | — | Text Qualitative | 3 · 2.2 Quantitative Comparison with Experiment · Figure 2a |
| PXRD peak positions | 4.7, 9.4, 12.5, 16.4 and minor 27.1 degrees 2theta | — | — | Text Rounded Reported | 3 · 2.2 Quantitative Comparison with Experiment · Figure 2a |