SEM and TEM
near-ideal Ni3(HITP)2 crystallite powder · Powder
SEM on ZEISS GeminiSEM 300 at 3 kV; HR-TEM on FEI Tecnai G2 20 at 200 kV; TEM samples drop-cast on Cu grids from methanol dispersion.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | rod-like crystallite | — | — | Caption Qualitative | 8 · Supplementary Note 3 · Figure S8 |
| TEM pore packing | well-defined hexagonal pore packing | — | — | Caption Qualitative | 8 · Supplementary Note 3 · Figure S8 |