Microscopy Morphology — Nanostructured Conductive Metal Organic Frameworks for Sustainable Low Charge Overpotentials in Li–Air Batteries

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

discharged Cu-THQ/GDE cathode · Electrode

Cu-THQ cathode after 10th discharge at 2 A/g; TEM samples sonicated 15 min in acetonitrile and drop-cast on holey carbon coated copper grids

Geometry: discharged cathode and TEM grid
Context: discharge product on c-MOF cathode
Measurement source: 4 · 2.3. Characterization of Discharge Product · Figure 2d-f; Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Li2O2 product architectureMarked as a best value within this paper	nanocrystalline grains embedded in amorphous Li2O2	—	—	Text Qualitative	4 · 2.3. Characterization of Discharge Product · Figure 2e
Li2O2 nanocrystalline grain sizeMarked as a best value within this paper	2-5 nm	—	range	Text Range	4 · 2.3. Characterization of Discharge Product · Figure 2e

Cu-THQ nanoflakes · Nanosheet

Cu-THQ NFs dispersed in IPA at 25 C; Malvern Zetasizer Nano ZSP, 633 nm laser

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
average nanoflake lateral sizeMarked as a best value within this paper	145 nm	—	—	Text Exact Reported	2 · 2.1. Cu-THQ Nanoflakes Characterization · Figure 1a

Cu-THQ nanoflakes · Nanosheet

JEOL JEM2100 at 200 kV; nanoflake suspension on carbon-coated copper grid

Geometry: TEM grid
Context: pristine c-MOF nanoflakes
Measurement source: 2 · 2.1. Cu-THQ Nanoflakes Characterization · Figure 1c-e

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HRTEM d020 spacing	d020 = 1.10 nm	—	—	Text Exact Reported	2 · 2.1. Cu-THQ Nanoflakes Characterization · Figure 1c-e
HRTEM d110 spacing	d110 = 1.13 nm	—	—	Text Exact Reported	2 · 2.1. Cu-THQ Nanoflakes Characterization · Figure 1c-e
open pore size	smaller than 1 nm	—	<	Text Approximate	2 · 2.1. Cu-THQ Nanoflakes Characterization · Figure 1c-e