Synthesis · Nanostructured Conductive Metal Organic Frameworks for Sustainable Low Charge Overpotentials in Li–Air Batteries

2 structured synthesis routes

Completeness describes how fully the route could be reconstructed from the main article and supporting information.

Partial recipeSource: Main

7 · Experimental Section, Cathode Preparation

Metal precursorsCu-THQ NFs

Linker precursorstetrahydroxyquinone present in Cu-THQ NFs

Solventsnot specified for coating step

Atmospherenot specified for coating; battery assembled in argon-filled glovebox

Substrate orientation1 cm2 GDE (Sigracet 25 BC)

Work-up100 mg Cu-THQ NFs coated on 1 cm2 GDE

Show 2 structured reagent records

Role	Reagent	Amount / concentration	Source
Other	Cu-THQ NFs	100 mg	7 · Experimental Section, Cathode Preparation
Other	GDE (Sigracet 25 BC)	1 cm2	7 · Experimental Section, Cathode Preparation

Partial recipeSource: Both

2 · S1. Synthesis of Cu-THQ Nano-flakes (NFs)

Metal precursorspre-synthesised bulk Cu-THQ powder

Linker precursorscontained in pre-synthesised Cu-THQ powder; tetrahydroxyquinone linker not separately used in this route

Solventsisopropyl alcohol (IPA), 12 mL

Atmospherenot specified

Time4 h sonication; 1 h centrifugation

Work-upprobe sonication (Vibra Cell Sonics 130 W) for 4 h; centrifuge 60 min at 2000 rpm; collect supernatant

Show 2 structured reagent records

Role	Reagent	Amount / concentration	Source
Other	Cu-THQ powder	30 mg	2 · S1. Synthesis of Cu-THQ Nano-flakes (NFs)
Solvent	isopropyl alcohol (IPA)	12 mL	2 · S1. Synthesis of Cu-THQ Nano-flakes (NFs)