Spectroscopy — Electrochemical investigation of copper 1D conductive polymer for hybrid supercapacitor applications

Measurement evidence

Spectroscopy

Electrochemical investigation of copper 1D conductive polymer for hybrid supercapacitor applications · Shah J.H., Sharif S., Shahbaz M. et al. · Journal of Energy Storage · 2024 · 114058

3 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR, ATR compartment, Bruker Tensor-27

Cu-PDA-MOF blue crystals · Single Crystal

400-4000 cm-1 range; comparison with free 2,6-PDA ligand.

Context
pristine Cu-PDA-MOF crystals
Measurement source
office text · FTIR & Thermal Analysis · Figs. S1-S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-PDA-MOF asymmetric carboxylate stretch1618 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S1
Cu-PDA-MOF asymmetric carboxylate stretch1597 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S1
Cu-PDA-MOF symmetric carboxylate stretch1436 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S1
Cu-PDA-MOF symmetric carboxylate stretch1364 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S1
O-H FTIR bandO-H at 3083 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S1

FTIR free-ligand control

Free 2,6-PDA ligand · Powder

FTIR comparison peaks for free 2,6-PDA ligand.

Context
free ligand model control
Measurement source
office text · FTIR & Thermal Analysis · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
free ligand carboxylate comparison peaks1691, 1572, 1455 and 1411 cm-1Text
Exact Reported
office text · FTIR & Thermal Analysis · Fig. S2

Thermogravimetric analysis

Cu-PDA-MOF blue crystals · Single Crystal

TA Instruments SDT Q600; 10 deg C min-1 ramp; N2 atmosphere; 25-1000 deg C.

Atmosphere
N2
Context
pristine Cu-PDA-MOF crystals
Measurement source
office text · FTIR & Thermal Analysis · Fig. S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thermal stability thresholdstable up to 130 C403.15 KText
Rounded Reported
office text · FTIR & Thermal Analysis · Fig. S3