Spectroscopy — A Triptycene-Based Layered/Flower-Like 2D Conductive Metal–Organic Framework with 3D Extension as an Electrode for Efficient Li Storage

Measurement evidence

Spectroscopy

A Triptycene-Based Layered/Flower-Like 2D Conductive Metal–Organic Framework with 3D Extension as an Electrode for Efficient Li Storage · Liu X., Yu M., Liu J. et al. · Small · 2024 · 2306159

1 measurement group · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR, EPR, XPS

Infrared spectroscopy X-ray photoelectron spectroscopy Electron paramagnetic resonance

Pristine M-DBH powders (M = Ni, Co, Mn) · Powder

FTIR-ATR 400-4000 cm^-1; EPR at room temperature; XPS with Al K alpha radiation.

Temperature: 298
Context: Pristine M-DBH powders
Measurement source: p004-p005 · Results and Discussion 2.1 · Figures 2-3; Tables S2-S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
EPR g factor	g = 2.01	—	—	Text Exact Reported	p004 · Results and Discussion 2.1 · Figure 2e
FTIR characteristic bands of M-DBH	877, 1047, and 1340 cm^-1	—	—	Text Rounded Reported	p004 · Results and Discussion 2.1 · Figure 2f
Thermal stability threshold	good thermal stability below 180 deg C	—	below	Text Rounded Reported	p004 · Results and Discussion 2.1 · Figure 2d
Co-DBH Co 2p3/2 binding energy	780.07 eV	—	—	SI Table Exact Reported	p014 · 5. Supporting Table · Table S4
Mn-DBH Mn 2p3/2 binding energy	640.84 eV	—	—	SI Table Exact Reported	p014 · 5. Supporting Table · Table S3
Ni-DBH Ni 2p3/2 binding energy	855.56 eV	—	—	SI Table Exact Reported	p013 · 5. Supporting Table · Table S2