Microscopy Morphology — Controlling the Spatiotemporal Self-Organization of Stimuli-Responsive Nanocrystals under Out-of-Equilibrium Conditions

Measurement evidence

Microscopy Morphology

Controlling the Spatiotemporal Self-Organization of Stimuli-Responsive Nanocrystals under Out-of-Equilibrium Conditions · Damacet P., Shehayeb E.O., Mirica K.A. · Journal of the American Chemical Society · 2025 · 1584-1594

2 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and ImageJ particle size analysis

1D reaction-diffusion Ni3(HITP)2 Liesegang precipitation zones · Powder

SEM on Thermo Scientific Helios 5 CX DualBeam; ImageJ analysis of particles from each zone.

Context
pristine RD-derived framework particles
Measurement source
1588 · 3.2 Morphological Features · Figure 3c,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
1D particles 4 cm comparison length1.1 +/- 0.2 um+/- 0.2 umText
Rounded Reported
1589 · 3.4 2D Liesegang Rings · Figures S75-S77
1D interface particle length-to-width aspect ratio3.7Text
Rounded Reported
1588 · 3.2 Morphological Features · Figure 3
1D Zone 5 particle length-to-width aspect ratio6.8Text
Rounded Reported
1588 · 3.2 Morphological Features · Figure 3

SEM and ImageJ particle size analysis

2D RD Ni3(HITP)2 Zone 3 particles · Powder

Particle size distribution determined from 70 particles from each 2D zone.

Context
pristine 2D RD-derived framework particles
Measurement source
1588 · Figure caption · Figure 4f,g
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
2D particles 4 cm from junction length3.3 +/- 0.6 um+/- 0.6 umText
Rounded Reported
1589 · 3.4 2D Liesegang Rings · Figures S75-S77
2D interface particle aspect ratio for sensing4.6 +/- 0.5+/- 0.5Text
Rounded Reported
1590 · 3.5 Chemiresistive Detection · Figure 5b,d
2D Zone 3 particle aspect ratio for sensing8.2 +/- 0.4+/- 0.4Text
Rounded Reported
1590 · 3.5 Chemiresistive Detection · Figure 5b,d