cMOF Evidence Base
Porosity — Facile synthesis of Ni-, Co-, Cu-metal organic frameworks electrocatalyst boosting for hydrogen evolution reaction

Measurement evidence

Porosity

Facile synthesis of Ni-, Co-, Cu-metal organic frameworks electrocatalyst boosting for hydrogen evolution reaction · Zhang M., Hu D., Xu Z. et al. · Journal of Materials Science and Technology · 2021 · 172-179

3 measurement groups · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 adsorption-desorption and NLDFT pore-size analysis

Gas sorption and porosity

As-prepared Co-BTC crystals/powder · Powder

Nitrogen adsorption-desorption isotherm at 77 K with automated gas sorption analyser; NLDFT/Tarazona model for pore-size distributions.

Temperature
77
Atmosphere
N2
Context
pristine powder
Measurement source
main p.4, article p.175 · Results and discussion · Fig. 3c,d; Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average pore diameter3.65 nm——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Micropore volume0.198 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Specific surface area436.2 m2 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Total pore volume0.401 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1

N2 adsorption-desorption and NLDFT pore-size analysis

Gas sorption and porosity

As-prepared Cu-BTC blue crystals/powder · Powder

Nitrogen adsorption-desorption isotherm at 77 K with automated gas sorption analyser; NLDFT/Tarazona model for pore-size distributions.

Temperature
77
Atmosphere
N2
Context
pristine powder
Measurement source
SI text p.1 · Characterization · Fig. 3c,d; Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average pore diameter3.66 nm——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Micropore volume0.125 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Specific surface area395.3 m2 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Total pore volume0.361 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1

N2 adsorption-desorption and NLDFT pore-size analysis

Gas sorption and porosity

As-prepared Ni-BTC precipitate/powder · Powder

Nitrogen adsorption-desorption isotherm at 77 K with automated gas sorption analyser; NLDFT/Tarazona model for pore-size distributions.

Temperature
77
Atmosphere
N2
Context
pristine powder
Measurement source
main p.4, article p.175 · Results and discussion · Fig. 3c,d; Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average pore diameter of fabricated MOFs~3.7 nm—~Text
Approximate		main p.4, article p.175 · Results and discussion · Fig. 3d; Table S1
Average pore diameterMarked as a best value within this paper3.75 nm——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Micropore volumeMarked as a best value within this paper0.271 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Specific surface areaMarked as a best value within this paper506.4 m2 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1
Total pore volumeMarked as a best value within this paper0.542 cm3 g-1——SI Table
Exact Reported		SI rendered p.12 (S12) · Table S1 · Table S1