Microscopy Morphology — Conductive Metal-Organic Frameworks Bearing M−O4 Active Sites as Highly Active Biomass Valorization Electrocatalysts

Measurement evidence

Microscopy Morphology

Conductive Metal-Organic Frameworks Bearing M−O4 Active Sites as Highly Active Biomass Valorization Electrocatalysts · Zhang Y., Kornienko N. · ChemSusChem · 2022 · e202101587

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM top-view and cross-section

Ni-CAT-FTO · Electrode

SEM images of Ni-CAT-FTO after growth.

Geometry
film on FTO
Context
Composite electrode sample
Measurement source
3 · Results and Discussion · Figure 2c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
MOF surface coveragesurface is covered with MOF crystalsQualitative
Qualitative
3 · Results and Discussion · Figure 2c and Figure S1
Ni-CAT-FTO film thicknessabout 220 nmText
Approximate
3 · Results and Discussion · Figure 2c inset

TEM

Ni-CAT-FTO · Electrode

TEM of particles scratched from FTO films, dispersed in ethanol and deposited on copper grids.

Geometry
scratched film particles
Context
Composite electrode material isolated for TEM
Measurement source
3 · Results and Discussion · Figure 2d and Figure S1d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TEM pore morphologyhexagonal pores within the samplesQualitative
Qualitative
3 · Results and Discussion · Figure 2d and Figure S1d