Thermogravimetric analysis
As-made Ga9(HOTP)4 microcrystalline powder · Powder
TA Instruments Q500; heating rate 3.0 deg/min under nitrogen gas flow of 5 ml/min on a platinum pan.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Framework decomposition range lower bound | around 250 C | 523.15 K | around | Text Range | SI p.2 · Elemental and thermogravimetric analysis · Figure S1 |
| Framework decomposition range upper bound | around 450 C | 723.15 K | around | Text Range | SI p.2 · Elemental and thermogravimetric analysis · Figure S1 |
| Low-temperature TGA derivative peaks | first two derivative mass-change peaks below 100 C | 373.15 K | below 100 C | Text Approximate | SI p.2 · Elemental and thermogravimetric analysis · Figure S1 |