Microscopy Morphology — Conjugated Nonplanar Copper-Catecholate Conductive Metal-Organic Frameworks via Contorted Hexabenzocoronene Ligands for Electrical Conduction

Measurement evidence

Microscopy Morphology

Conjugated Nonplanar Copper-Catecholate Conductive Metal-Organic Frameworks via Contorted Hexabenzocoronene Ligands for Electrical Conduction · Xing G., Liu J., Zhou Y. et al. · Journal of the American Chemical Society · 2023 · 8979-8987

6 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HRTEM and SAED

c-HBC-12O-Cu black powder · Powder

JEM-2100Plus at 200 kV; SAED along c axis.

Context
pristine framework powder
Measurement source
p005 / article p8983 · Results and Discussion · Figure 3e,f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SAED d020 spacingd020 = 1.38 nmText
Exact Reported
p005 / article p8983 · Results and Discussion · Figure 3f
SAED d200 spacingd200 = 0.79 nmText
Exact Reported
p005 / article p8983 · Results and Discussion · Figure 3f

FE-SEM

c-HBC-12O-Cu black powder · Powder

Hitachi SU8010, 5.0 kV.

Context
pristine framework powder
Measurement source
p004 / article p8982 · Results and Discussion · Figure S12
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM morphologynanowire morphologyText
Qualitative
p004 / article p8982 · Results and Discussion · Figure S12

HRTEM and SAED

c-HBC-6O-Cu black powder · Powder

JEM-2100Plus at 200 kV; images along pore direction with model overlay.

Context
pristine framework powder
Measurement source
p004 / article p8982 · Results and Discussion · Figure 3a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SAED/HRTEM d110 spacingd110 = 1.35 nmVisual Estimate
Approximate
p004 / article p8982 · Results and Discussion · Figure 3a
SAED/HRTEM d2-10 spacingd2-10 = 1.35 nmVisual Estimate
Approximate
p004 / article p8982 · Results and Discussion · Figure 3a

FE-SEM

c-HBC-6O-Cu black powder · Powder

Hitachi SU8010, 5.0 kV.

Context
pristine framework powder
Measurement source
p004 / article p8982 · Results and Discussion · Figure S12
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM morphologylamellar morphologyText
Qualitative
p004 / article p8982 · Results and Discussion · Figure S12

HRTEM and SAED

c-HBC-8O-Cu black powder · Powder

JEM-2100Plus at 200 kV; SAED along c axis.

Context
pristine framework powder
Measurement source
p005 / article p8983 · Results and Discussion · Figure 3c,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SAED d020 spacingd020 = 1.39 nmText
Exact Reported
p005 / article p8983 · Results and Discussion · Figure 3d
SAED d200 spacingd200 = 0.82 nmText
Exact Reported
p005 / article p8983 · Results and Discussion · Figure 3d

FE-SEM

c-HBC-8O-Cu black powder · Powder

Hitachi SU8010, 5.0 kV.

Context
pristine framework powder
Measurement source
p004 / article p8982 · Results and Discussion · Figure S12
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM morphologyrod-like morphologyText
Qualitative
p004 / article p8982 · Results and Discussion · Figure S12