Diffraction Structure — Conductive Metal-Organic Frameworks for Amperometric Sensing of Paracetamol

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

As-synthesised NiCu-CAT nanocrystals · Powder

Rigaku D/max-2550 diffractometer with Cu Kalpha radiation, lambda = 1.5418 Angstrom; compared with simulated NiCu-CAT pattern.

Geometry: Powder/nanocrystal sample
Context: Pristine mixed-metal NiCu-CAT framework.
Measurement source: main pp.3-5 · Instrumentation; Results - Characterization · Figure 1D

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Long-range order in ab-plane	PXRD peaks indicate long-range order of the nanocrystal in the ab-plane	—	—	Text Qualitative	main p.5 · Results - Characterization · Figure 1D
PXRD (100) peak position	2theta = 4.7 deg	—	—	Text Rounded Reported	main p.5 · Results - Characterization · Figure 1D
PXRD (200) peak position	2theta = 9.5 deg	—	—	Text Rounded Reported	main p.5 · Results - Characterization · Figure 1D
PXRD (210) peak position	2theta = 12.4 deg	—	—	Text Rounded Reported	main p.5 · Results - Characterization · Figure 1D

NiCu-CAT/GCE after air storage for 7-30 days · Electrode

XRD pattern after pretreatment during 30 days; rendered Supplementary Figure 6 compares traces labelled 7 d and 30 d.

Atmosphere: Stored in air before measurement, as described for stability testing.
Geometry: Stored NiCu-CAT/GCE / NiCu-CAT sample state; geometry not otherwise specified.
Context: Stability check for NiCu-CAT-containing electrode/material after air storage.
Measurement source: SI p.3 · Supplementary Figures · Supplementary Figure 6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
XRD pattern retained after 7 and 30 days	7 d and 30 d XRD traces show the same principal low-angle and ca. 28 deg peaks by visual inspection	—	—	Visual Estimate Qualitative	SI p.3 · Supplementary Figures · Supplementary Figure 6