Powder X-ray diffraction, Bruker D8 Advance, Cu Kalpha radiation
Bulk Ni3(HITP)2 black powder · Powder
PXRD used to validate structure and purity of obtained black powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD peak positions matching Ni3(HITP)2 | 2theta = 4.7, 9.5, 12.6, 16.5 and 27.3 degrees | — | — | Text Exact Reported | main p.3, article p.341 · Results and discussion · Fig. 1b |