Other — Solvent-Directed Assembly of π-Stacked 3D Metal-Organic Frameworks with Tunable Conductivity Enhanced by C60 Encapsulation

Measurement evidence

Other

Solvent-Directed Assembly of π-Stacked 3D Metal-Organic Frameworks with Tunable Conductivity Enhanced by C60 Encapsulation · Tang X., Wang X., Su S. et al. · Journal of the American Chemical Society · 2025 · 20899-20908

2 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

ICP-OES

Bulk elemental and compositional analysis

NU-4003-C60 · Single Crystal

C60 mass fraction and channel occupancy determined after toluene washing

Measurement source: main p006-p007 / journal p20904-p20905 · Electrical Conductivity

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C60 channel occupancy	25% channel volume	—	—	Text Rounded Reported	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 mass fraction	approximately 13 wt %	—	—	Text Approximate	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 channel occupancy	36% channel volume	—	—	Text Rounded Reported	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 mass fraction	17 wt %	—	—	Text Rounded Reported	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 channel occupancy	54% channel volume	—	—	Text Rounded Reported	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 mass fraction	24 wt %	—	—	Text Rounded Reported	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 channel occupancy	approximately all pore volume occupied	—	—	Text Approximate	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4
C60 mass fraction	about 38 wt %	—	—	Text Approximate	main p006-p007 / journal p20904-p20905 · Electrical Conductivity · Figure 2; Figure 4

thermogravimetric analysis

Thermogravimetric analysis

NU-4003 · Single Crystal

25-600 C at 5 C/min under air; comparison of NU-4000-NU-4003 and NU-4003-C60

Atmosphere: air
Measurement source: SI p002 / S2 · Materials and General Procedures · Figure S18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TGA thermal event	NU-4003-C60 gradual decline between 300 and 550 C	—	—	Text Range	main p002-p006 / journal p20900-p20904 · Synthesis and Structural Characterization / Electrical Conductivity · Figure S18
TGA thermal event	NU-4003 decomposition begins at approximately 300 C under air	—	—	Text Approximate	main p002-p006 / journal p20900-p20904 · Synthesis and Structural Characterization / Electrical Conductivity · Figure S18