Diffraction Structure — Vertical Conductive Metal–Organic Framework Single-Crystalline Nanowire Arrays for Efficient Electrocatalytic Hydrogen Evolution

Measurement evidence

Diffraction Structure

Vertical Conductive Metal–Organic Framework Single-Crystalline Nanowire Arrays for Efficient Electrocatalytic Hydrogen Evolution · Dong J., Chi K., Zhao Y. et al. · Small · 2024 · 2404808

1 measurement group · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD (Bruker D8 Advance, Cu Kalpha) and synchrotron GIXRD/GIWAXS (lambda = 1.24 A, BL14B)

X-ray diffraction and scattering

Ag-MOF-NWs powder · Powder

Collected Ag-MOF-NWs powder and Ag-MOF-NWs on Si/SiO2 substrate used to assess crystallinity and ordered arrangement.

Geometry: powder and Si/SiO2-supported nanowire film
Context: pristine target sample
Measurement source: Supplementary Methods 1.5 Materials characterization

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag-BHT-NWs unit-cell volume	V = 550.978 A3	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Ag-BHT-NWs crystal system	Monoclinic	—	—	SI Table Qualitative	14 · Supplementary Tables · Table S1
Ag-BHT-NWs formula weight	803.80	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
GIWAXS/GIXRD crystallinity	pronounced diffraction ring; integral plot consistent with PXRD	—	—	Text Qualitative	4 · Synthesis and Characterization of Materials · Figure 4d,e
Pawley lattice parameter a	a = 15.1751 A	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley lattice parameter b	b = 9.0826 A	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley lattice parameter beta	beta = 110.4170 deg	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley lattice parameter c	c = 4.2655 A	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley/Rietveld refinement GOF	GOF = 1.52	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley refinement Rp	Rp = 2.031%	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
Pawley refinement Rwp	Rwp = 2.577%	—	—	SI Table Exact Reported	14 · Supplementary Tables · Table S1
PXRD peak positions	2theta approx. 11.3, 12.3, 20.5, 23.2, 24.0, 24.8, 31.3, 35.1 degrees	—	—	Text Approximate	4 · Synthesis and Characterization of Materials · Figure 4b
Ag-BHT-NWs space group	I2/m	—	—	SI Table Qualitative	14 · Supplementary Tables · Table S1