Microscopy Morphology — Vertical Conductive Metal–Organic Framework Single-Crystalline Nanowire Arrays for Efficient Electrocatalytic Hydrogen Evolution

Measurement evidence

Microscopy Morphology

Vertical Conductive Metal–Organic Framework Single-Crystalline Nanowire Arrays for Efficient Electrocatalytic Hydrogen Evolution · Dong J., Chi K., Zhao Y. et al. · Small · 2024 · 2404808

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM (SU8010) top-view and cross-sectional imaging

Ag-MOF-NWs · Single Crystal

Morphology comparison of Ag-MOF-Film, Ag-MOF-MWs and Ag-MOF-NWs formed after different reaction times.

Context
pristine morphology series
Measurement source
Supplementary Methods 1.5 Materials characterization
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag-MOF-NWs mean nanowire lengthapprox. 1 umText
Approximate
3 · Synthesis and Characterization of Materials · Figure 2c,f

TEM/HRTEM (JEM-2100), SAED and TEM-EDX elemental mapping

Ag-MOF-NWs powder · Powder

Ultrasonically dispersed Ag-MOF nanowires characterised for dimensions, lattice fringes, diffraction and elemental distribution.

Geometry
dispersed nanowires
Context
pristine target sample
Measurement source
Supplementary Methods 1.5 Materials characterization
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TEM-EDX elemental distributionhomogeneous sulfur and silver distributionText
Qualitative
3 · Synthesis and Characterization of Materials · Figure 3e
HRTEM lattice fringe assigned to (10-1)0.43 nmText
Exact Reported
3 · Synthesis and Characterization of Materials · Figure 3b
HRTEM lattice fringe assigned to (110)0.78 nmText
Exact Reported
3 · Synthesis and Characterization of Materials · Figure 3b
Ag-MOF-NWs prism diameterof the order of 100 nmText
Approximate
3 · Synthesis and Characterization of Materials · Figure 3a
Ag-MOF-NWs TEM lengthapproximate length of 1 umText
Approximate
3 · Synthesis and Characterization of Materials · Figure 3a
SAED single-crystalline characterbright diffraction points aligned with simulated diffraction patternText
Qualitative
3 · Synthesis and Characterization of Materials · Figure 3c,d