SEM and HRTEM
Ni3(THT)2 black powder · Powder
SEM on Carl Zeiss Merlin at 5.00 kV; TEM on FEI Tecnai F30 after dispersing powder in MeCN and sonicating about 5 min
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| HRTEM/FFT d(100) spacing | 1.99 nm | — | — | Text Rounded Reported | 3 · Results and Discussion · Figure 2C |
| HRTEM crystalline domain size | ~100's of nms | — | — | Text Approximate | 3 · Results and Discussion · Figure 2C; Figure S7 |
| SEM morphology | sheet-like morphology | — | — | Text Qualitative | 3 · Results and Discussion · Figure 2C |