PXRD and SEM
NiCB@NU-1000 powder · Powder
Powder XRD patterns compared with simulated NU-1000; SEM image of NiCB@NU-1000.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
Diffraction Structure — Increased Electrical Conductivity in a Mesoporous Metal-Organic Framework Featuring Metallacarboranes Guests
Measurement evidence
Diffraction Structure
Increased Electrical Conductivity in a Mesoporous Metal-Organic Framework Featuring Metallacarboranes Guests · Kung C.-W., Otake K., Buru C.T. et al. · Journal of the American Chemical Society · 2018 · 3871-3875
2 measurement groups · 7 results
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
single-crystal X-ray diffraction
NiCB@SC-NU-1000 single crystal · Single Crystal
One crystal mounted in paratone oil and measured at 100 K with Mo Kalpha radiation; SQUEEZE used for disordered solvent.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| a lattice parameter | 38.555(4) A | — | (4) | SI Table Exact Reported | S11 · S4 · Table S2 |
| c lattice parameter | 17.061(2) A | — | (2) | SI Table Exact Reported | S11 · S4 · Table S2 |
| Single-crystal ICP loading | 0.71 Ni on each Zr6 node | — | — | Text Exact Reported | S9 · S4 |
| Crystallographic NiCB loading | 0.667 NiCB on each Zr6 node | — | — | Text Exact Reported | S9 · S4 · Figure S3 |
| Ni site occupancy | 100% | — | — | Text Exact Reported | S9 · S4 · Figure S3 |
| Space group | P6/mmm (no.191) | — | — | SI Table Exact Reported | S11 · S4 · Table S2 |
| Unit-cell volume | 21962(5) A3 | — | (5) | SI Table Exact Reported | S11 · S4 · Table S2 |