Diffraction Structure — Microwave discharge for rapid introduction of bimetallic-synergistic configuration to conductive catecholate toward long-term supercapacitor

Measurement evidence

Diffraction Structure

Microwave discharge for rapid introduction of bimetallic-synergistic configuration to conductive catecholate toward long-term supercapacitor · Jiang H., Xian J., Hu R. et al. · Chemical Engineering Journal · 2023 · 140804

1 measurement group · 19 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XRD with Cu-Kalpha radiation and XPS

X-ray photoelectron spectroscopy X-ray diffraction and scattering

Zn,Ni-CAT-T4 · Electrode

XRD measured at 40 kV and 40 mA; XPS used to analyse surface species and chemical states.

Geometry: Supported Zn,Ni-CAT electrode
Context: Target mixed-metal MOF compared against pristine Ni-CAT.
Measurement source: 2 · 2.6. Characterization · Figure 2f-i

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni-CAT Ni 2p1/2 binding energy	874.23 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Ni-CAT Ni 2p3/2 binding energy	856.12 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Ni-CAT Ni 2p satellite binding energy 1	861.56 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Ni-CAT Ni 2p satellite binding energy 2	880.20 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Zn,Ni-CAT (100) XRD peak shift versus Ni-CAT	Delta theta = 0.39 degrees to lower diffraction angle	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2f
C 1s C=C binding energy	284.80 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2g
C 1s C=O/C-O binding energy assignment 1	286.34 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
C 1s C-O binding energy assignment 2	288.43 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
*C 1s pi-pi satellite binding energy**	290.84 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Zn,Ni-CAT Ni 2p1/2 binding energy	873.92 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2h
Zn,Ni-CAT Ni 2p1/2 negative shift versus Ni-CAT	-0.31 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Zn,Ni-CAT Ni 2p3/2 binding energy	855.80 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2h
Zn,Ni-CAT Ni 2p3/2 negative shift versus Ni-CAT	-0.32 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
O 1s C-O binding energy	533.12 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
O 1s H2O binding energy	535.75 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
O 1s metal-oxygen binding energy	531.44 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4
Zn,Ni-CAT Zn 2p1/2 binding energy	1044.92 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2i
Zn,Ni-CAT Zn 2p3/2 binding energy	1021.74 eV	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2i
Zn oxidation state in Zn,Ni-CAT	Zn exists as Zn2+	—	—	Text Qualitative	4 · 3.1. Synthesis and characterization · Figure 2 and Figure S4