Microscopy Morphology — Microwave discharge for rapid introduction of bimetallic-synergistic configuration to conductive catecholate toward long-term supercapacitor

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Zn,Ni-CAT-T4 · Electrode

Morphology and elemental distribution of Zn,Ni-CAT nanorods grown on carbon cloth.

Geometry: Carbon cloth supported nanorod electrode
Context: Target microwave-treated mixed-metal MOF compared with pristine Ni-CAT morphology through SI reference.
Measurement source: 4 · 3.1. Synthesis and characterization · Figure 2a-e

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Original Ni-CAT (100) lattice spacing	1.77 nm	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2d
Zn,Ni-CAT (100) lattice spacing	1.85 nm	—	—	Text Exact Reported	4 · 3.1. Synthesis and characterization · Figure 2d
Zn,Ni-CAT morphology	Zn,Ni-CAT nanorods grow uniformly on the surface of carbon fiber	—	—	Text Qualitative	4 · 3.1. Synthesis and characterization · Figure 2a-b

Zn,Ni-CAT treated for 25 s · Electrode

Morphology comparison for overlong microwave reaction times shown in SI Figure S7.

Context: Mixed-metal Zn,Ni-CAT on carbon cloth compared with T1-T4 pulse-series samples.
Measurement source: 5 · Fig. S1 to S23 · Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Zn,Ni-CAT 25 s morphology	partially damaged at 25 s	—	—	Text Qualitative	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure S7

Zn,Ni-CAT treated for 60 s · Electrode

Morphology comparison for overlong microwave reaction times shown in SI Figure S7.

Context: Mixed-metal Zn,Ni-CAT on carbon cloth compared with T1-T4 pulse-series samples.
Measurement source: 5 · Fig. S1 to S23 · Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Zn,Ni-CAT 60 s morphology	significantly collapsed at 60 s	—	—	Text Qualitative	6 · 3.3. Optimization of bimetallic MOFs by microwave · Figure S7

Glass after Zn-wire microwave discharge control · Thin Film

Control experiments using glass or carbon cloth under comparable Zn-wire microwave discharge conditions.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Carbon-cloth control Zn deposition	None of Zinc; carbon 100 wt%	—	—	Figure Axis Qualitative	5 · Figure 3 · Figure 3e
Glass-control Zn content after microwave discharge	Zn 30.45 wt%	—	—	Figure Axis Rounded Reported	5 · Figure 3 · Figure 3c